Structural, Optical, and Antibacterial Properties of Nanocomposite Synthesized by a Facile Microplasma Electrochemical Process

Volume: 10 | Issue: 02 | Year 24 | Subscription

Received Date: 10/10/2024
Acceptance Date: 10/14/2024
Published On: 2024-10-14
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By: Afaq Khaliq and Muhammad Nabeel Sharif

1. Student, Nano-Scale Physics Laboratory, Department of Physics, Air University, Islamabad, Pakistan

2.Student, Department of Physics, University of Poonch Rawalakot, Rawalakot 12350, Pakistan

Abstract

Nowadays increasing severity of environmental pollution and antibiotic resistance poses significant global challenges, particularly due to the accumulation of organic pollutants from industrialization and the proliferation of antibiotic-resistant bacteria, which jeopardize ecosystems and public health. To address these issues, the development of advanced nanocomposites with photocatalytic and antimicrobial properties is of paramount importance. This article reports the synthesis of nanocomposite conducted in the current study via atmospheric pressure microplasma (AMP) electrochemical method.The synthesized nanocomposite’s optical, structural, morphological, and compositional characteristics were thoroughly examined using UV-visible spectroscopy, X-ray diffraction (XRD), SEM, and Fourier-transform infrared (FTIR) spectroscopy. XRD analysis confirmed the crystalline structure of the nanocomposite, indicating the presence of a cubic spinel phase of  (space group Fd-3m) and a cubic phase of , with a crystallite size of 24.2 nm. SEM analysis demonstrated that nanocomposite exhibited a spherical-like morphology. FTIR spectra showed characteristic metal-oxygen ( ) stretching vibrations at  and . UV-visible absorption spectra revealed a broad absorption peak at , and the nanomaterial’s optical energy bandgap was estimated to be 2.4 eV. These findings highlight the potential of the  nanocomposite for applications in environmental remediation and antimicrobial treatments.

Keywords: Nickel chromite, Atmospheric pressure microplasma, Spinel structure.

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