2 publications
-
Published Subscription
Green Synthesis, Characterization and Antimicrobial Studies of Ni(II) and Cu(II) Schiff Base ComplexesBy Salihu Sani
Abstract: Solvent-assisted mechanochemical reaction was used to synthesize new transition metal complexes of Ni(II) and Cu(II) with Schiff base ligand (H2L) obtained from condensation of 2-hydroxy-1- napthaldehyde with 2 aminobenzimidazole. Melting point/decomposition temperature, solubility test, FT-IR, powder x-ray analysis, conductivity measurement, magnetic susceptibility, elemental microanalysis, and UV/VIS spectral investigations were used to characterize the Schiff base and complexes. The complexes are of varied colours and have sharp melting points, and they …
Published in International Journal of Green Chemistry · Vol. 8, Issue 1, 2022 · pp. 9–18 Read article →
-
Published Subscription
Green Synthesis of Nickel(II) and Zinc(II) Complexes of Bis(Imine) Schiff base Derived from o-vanilline and m-phenylenediamine.By Salihu Sani, Ibrahim Tajo Siraj, Muktar Atiku Kurawa
Abstract: The synthesis of Schiff base ligand derived from aromatic aldehyde (o-vanillin) and m-phenylenediamine via liquid-assisted mechanochemical synthesis (LAG) in the presence of small amount of dimethylformamide were reported. The Schiff base complexes of Ni(II) and Zn(II) were also synthesized mechanochemically and characterized using infra-red spectroscopy, thermogrametric analysis, energy dispersive x-ray analysis, powder x-ray diffraction, UV-Visible analysis, conductivity measurement, magnetic susceptibility measurement and CHN, micro-analysis. Infrared spectral study indicated a strong …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 6, Issue 1, 2020 · pp. 31–43 Read article →