Volume: 12 | Issue: 1 | Year 2026 | Subscription
Received Date: 01/07/2026
Acceptance Date: 01/27/2026
Published On: 2026-02-10
First Page: 1
Last Page: 11
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By: Noor Sabah Muttaleb, Sara Abdalkareem Moshref, Safa Saleem Zayed, and Nagham Mahmood Aljamali.
1 Assist.Lecturer., Department of Chemistry, College of Education for Girls, University of Kufa, Iraq.
2Assist. Lecturer., Al-Furat Al-Awsat Technical University, Engineering Technical College of
Al-Najaf, 31001, Iraq
3Lecturer., Department of Chemistry, College of Education for Girls, University of Kufa, Iraq.
4*Professor., Department of Chemistry, College of Education, Iraq
Abstract
Due to the widespread pollution of heavy metals in water and environmental samples, the pollution levels have increased. Therefore, researchers have begun working on various environmental solutions to improve the levels of these elements in environmental samples. One such solution is the preparation of analytical reagents as coordination agents and ligands to shield the elements from water and soil, thereby reducing pollution levels. In this study, new analytical reagents were prepared from aniline compounds and others from azo compounds, which are known as analytical reagents with wide-ranging applications in analytical chemistry and biochemistry due to the presence of electron pairs in their hybrid atoms (nitrogen). After preparing the reagents, their precise chemical structures were determined through infrared spectroscopy, resonance spectroscopy, and ultraviolet spectroscopy. Additional studies were conducted, including the evaluation of their biological properties using a chemical analysis software program with Biological Tests.
Citation:
How to cite this article: Noor Sabah Muttaleb, Sara Abdalkareem Moshref, Safa Saleem Zayed, and Nagham Mahmood Aljamali Synthesis, Characterization, Antibacterial Study and Study of Bio Properties for New Analytical Reagents. International Journal of Environmental Chemistry. 2026; 12(1): 1-11p.
How to cite this URL: Noor Sabah Muttaleb, Sara Abdalkareem Moshref, Safa Saleem Zayed, and Nagham Mahmood Aljamali, Synthesis, Characterization, Antibacterial Study and Study of Bio Properties for New Analytical Reagents. International Journal of Environmental Chemistry. 2026; 12(1): 1-11p. Available from:https://journalspub.com/publication/ijec/article=23624
Refrences:
- Brüschweiler B J, Cédric M. Azo Dyes in Clothing Textiles Can Be Cleaved into a Series of Mutagenic Aromatic Amines Which Are Not Regulated Yet. Regulatory Toxicology and Pharmacology, 2017; 88(6): 214–226.
- Wu S, Liu J, Tan B, He C, Wu W, Yu L, Li Design, Synthesis, Antibacterial, and Antifungal Activity Evaluation of Novel Pyrimidine Derivatives Incorporating Amide and 1, 3, 4-Thiadiazole Thioether Moieties. Russian Journal of General Chemistry. 2024; 94(12): 3448-3455.
- Liu J, Bedell T, West J, Sorensen E. Design and Synthesis of Molecular Scaffolds with Anti-infective Activity . Tetrahedron. 2026; 72 (25): 3579–3592. doi:1016/j.tet.2016.01.044
- Mahmood N. Alternative Methods in Organic Synthesis. Eliva Press SRL. 2020; 1st Ed. ISBN: 9798680201176.
- Nagham M. The Various Preparation Methods in Synthetic Chemistry. Evincepub Publishing house. 2019; 1st Ed. ISBN: 978-93-88277-82-2.
- Alsbr I, Abdullabass H, Mahmood N. Invention of (Gluta.Sulfazane-Cefixime) Compounds as Inhibitors of Cancerous Tumors. Journal of Cardiovascular Disease Research. 2020; 11(2): 44-55.
- Mahmood N. Synthesis of Antifungal Chemical Compounds from Fluconazole with (Pharma-Chemical) Studying. Research journal of Pharmaceutical, biological and chemical sciences. 2017; 8(3): 564-573.
- Hall L, Hill D, Bugden K, Cawley S, Hall L, Chen M, Grant F. Development of a Reverse Phase Hplc Retention Index Model for Nontargeted Metabolomics Using Synthetic Compounds. Journal of Chemistry Inf Model.2018; 58(5): 591– 604.
- Tada R, Chavda N, Shah MK. Synthesis and characterization of some new thiosemicarbazide derivatives and their transition metal complexes. J Chem Pharm Res. 2011; 3: 290–297.
- Mahmood N. Synthesis and Biological Study of Hetero (Atoms and Cycles) Compounds., Der Pharma Chemica. 2016; 8(6): 40-48.
- Hasaneen K, Aseel M, Mahmood N. Synthesis of drugs derivatives as inhibitors of cancerous cells., Biochem. Cell. Arch. 2020; 20 (2): 82-96.
- Afaq J. Synthesis, Spectral Investigation and Study of Nano-Applications of New Anil-Azo Ligands., Al-Harf Journal. 2025; 24 (4): 28-39.
- Atheraa A. Studying of Thermal, Spectral and Liquid Crystal Properties of New Monomers for Schiff Base Reaction. Al-Harf 2024; 20(1) : 45-55.
- Rajaa A. Preparation and Characterization, and Study of Nano-Behaviour of New Benzothiazole and Triazole Derivatives. Al-Harf Journal. 2025; 24 (3): 73-87
- Alfatlawi I, Mahmood N, Nuha S, Zainab M. Synthesis of New Organic Compounds Via Three Components Reaction with Studying of (Identification, Thermal Behavior, Bioactivity on Bacteria of Teeth). Journal of Global Pharma Technology. 2017; 11(9): 157-164.
- Mahmood N, Saher M, Zainab M, Intisar O. Inhibition activity of (Azo–acetyl acetone) on bacteria of mouth., Research Journal of Pharmacy and Technology. 2017; 10(6):1683-1686.
- Jawad A, Mahmood N, Saher M. Development and Preparation of ciprofloxacin Drug Derivatives for Treatment of Microbial Contamination in Hospitals and Environment. Indian Journal of Forensic Medicine & Toxicology. 2020; 14(2): 1115-1122.
- Kalapala V, Banothu V, Chandra S. Synthesis and characterization of some new thiosemicarbazide derivatives and their transition metal complexes. Journal of Chem Pharm Res. 2015; 7(9): 437–445.
- Mahmood N. Synthesis and Chemical Identification of Macro Compounds of (Thiazol and Imidazol) .,Research J. Pharm. and Tech. 2015; 8(1): 78-84.
- Eva E, Heidi U, Rudolf V, Burkhard K, Michael L, Rudolf S, Wolfgang B. Azo Pigments and a Basal Cell Carcinoma at the Thumb . Dermatology. 2024; 216 (1): 76–80
- Nagham M. Survey on Methods of Preparation and Cyclization of Heterocycles. International Journal of Chemical and Molecular Engineering. 2020; 6(2): 19–36p.
- Braccia DJ, Minabou N, Weiss A, Levy S, Abeysinghe S, Jiang X, Pop M. Azo Drug Metabolism and Disposition. Science Research Journal. 2023; 51(5): 142–153.
- Naumann d, Raoul C, Lénárd H, Michael G . The reaction network in propane oxidation over phase-pure MoVTeNb M1 oxide catalysts . Journal of Catalysis .2014; 311(6): 369–385.
- Mahmood N. Survey on Semicarbazide and Thiosemicarbazide Derivatives. International Journal of Chemical Synthesis and Chemical Reaction. 2021; 7(1): 51–57
- Mahmood N. Review in Azo Compounds and its Biological Activity. Biochem Anal Biochem. 2015; 5(3): 169-176
- Nagham M. Creation of Originated Macrocyclic Sulfazan-Formazan Compounds and Linear Sulfazan-Formazan for the first Time Globally with their Assay as Antifungal. Biomedical Journal of Scientific & Technical Research. 2021; 40(3): 32266-32272 .
- Mokrani T, Van R, Albert A, Ismael . Molecular weight and tacticity effect on morphological and mechanical properties of Ziegler–Natta catalyzed isotactic polypropylenes. Polímeros. 2024; 25 (6):556–563.
- Shireen R, Mahmood N, Ali J. Guanine substituted heterocyclic derivatives as bioactive compounds., Biochem. Cell. Arch. 2020 20 (2): 3651-3655.
- Nagham A. Inventing of Macrocyclic Formazan Compounds and Studying Them Against Breast Cancer for The first Time Globally. Annals of pharma research. 2021; 9 (7): 525-533.
- Mahmood N ,Nemah S. Chemo – Spectral and Biological Studying of New Ligands . Research Journal of Pharmaceutical. Biological and Chemical Sciences. 2017 ;8(3) : 674-689.
- Mahmood N. Designation of Macrocyclic Sulfazan and Triazan as Originated Compounds with Their Estimation in Nano-Activities by the Scanning Microscope. International Journal of Convergence in Healthcare. 2022; 2(1): 25-34.
- Nagham A. Origination of Macrocyclic Formazan with Macrocyclic Sulfazan and Triazan as Originated Compounds and Compared Their efficiency Against Breast Cancer. Open Access Journal of Biomedical Science. 2022; 4(1) :52-67.
- Mahmood Synthesis Innovative Cyclic Formazan Compounds for the First Time and Evaluation of Their Biological Activity. International Journal of Polymer Science & Engineering . 2021; 7(2): 5–14.
- Brédas J, Persson K, Seshadri R. Computational design of functional materials. Chem Mater. 2017;29(6):2399-2401.
- Eftekhari B, Amirpour N, Naderahmadian A. Amphiphilic Azo-Functionalized Polyhedral Oligomeric Silsesquioxane; Synthesis and Photo-Switched Efficient Phase Transfer via Host–Guest Encapsulation . ChemPlusChem. 2024; 89 (5): 34-47.
- Nagham M. Inventing of Macrocyclic Formazan Compounds with Their Evaluation in Nano- Behavior in the Scanning Microscope and Chromatography. Biomedical Journal of Scientific & Technical Research. 2022; 41(3): 32783-32792
- Mahmood A, Zainab M. Anticancer Study of Innovative Macrocyclic Formazan Compounds from Trimethoprim Drug . Egyptian Journal of Chemistry . 2022 ;65(11): 31-44
- Zainab M, Mahmood A. Comparison of the efficiency of innovative formazan compound with innovative sulfazan against breast tumors. International Journal of Medicine Research. 2022; 7 (1):18-25
- Nadia E. Theoretical investigations of interactions between ruthenium (Ru) atoms and hydrogen (H) ligands in the di-bridged diruthenium cluster: [Cp*Ru(μ-H)4RuCp*]. Al-Harf Journal.2024; 20 (2): 71-86
- Zampaloni C, Mattei P, Bleicher K, Winther L, Thäte C, Bucher C. A novel antibiotic class targeting the lipopolysaccharide transporter”. Nature. 2024; 625 (7995): 566–571.
- Pahil K, Gilman M, Baidin V, Clairfeuille T, Mattei P, Bieniossek C. A new antibiotic traps lipopolysaccharide in its intermembrane transporter. Nature. 2024; 625 (7995): 572–577.