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475 articles for “Preparations”
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SYNTHESIS AND CHARACTERIZATION OF MIXED LIGAND COMPLEXES OF HYDROXAMIC ACIDS WITH POTASSIUM HEXATHIOCYANATO CHROMIUM (III) TETRA HYDRATE
Abstract: Some hydroxamic acids eg.[L1= benzohydroxamic acids (BHA), L2= N-phenyl– benzohydroxamic acid (NPBHA), L3= pivaloyl benzohydroxamic acid (PHA) and L4=N-phenyl-pivaloyl benzohydroxamic acid (PPHA) prepared and reacted with L’=Potassium hexathiocynato chromium (III) tetra hydrate K3[Cr(SCN)6]4H2O.The mixed ligand complexes of hydroxamic acids characterized with the help of repeated melting point, by I.R. studies, magnetic moment, molar conductance and by elemental analysis(C,H and N).The stoichiometry of the complexes were found to be 1:2(M:L) molar …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 2, Issue 2, 2016 Read article
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ISONIAZID STABILIZED TUNGSTEN TRICARBONYL COMPLEX: A NEW CO-RELEASING MOLECULE WITH ANTIBACTERIAL ACTIVITY
Abstract: Transition metal carbonyl complexes substituted with biologically active ligand can act as CO-releasing molecules which have beneficial roles including antimicrobial activity. Careful choices of ancillary ligand such as isoniazid help in eliminating issues of toxicity that may arise from drug substrates. Substitution reaction of tungsten hexacarbonyl with isoniazid in the presence of trimethylamine N-oxide under nitrogen atmosphere was carried out at ambient temperature for 72 hrs. The product was characterized …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 5, Issue 1, 2019 · pp. 36–43 Read article
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Short Report on Capillary Motion of Dyed Ethylene Glycol for Application towards the Gas Flow in Microfluidics
Abstract: In this experimental report, a couple of SU-8 based glass microfluidic devices are fabricated bymaskless lithography and indirect bonding technique. Each device is tested by the prepared dyedethylene glycol as working liquid. The microfluidic-leakage is recorded in the surface-drivencapillary motion of dyed ethylene glycol due to improper indirect bonding technique. The leakagefreesurface-driven capillary motion of dyed ethylene glycol is recorded due to proper indirectbonding technique. This experimental work is performed …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 7, Issue 1, 2021 · pp. 13–16 Read article
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Survey on Semicarbazide and Thiosemicarbazide Derivatives
Abstract: This review insurances around semicarbazide and thiosemicarbazide with derivatives throughpresentation of their preparation methods, reactions like cyclization processes. Thiosemicarbazonesand semicarbazones are an important class of ligands for the synthesis of transition metal complexeswith applications in medicine and electrochemistry, also in organic chemistry fields., Tumor is amalignant in addition invasive development or cancer, particularly of epithelium derivation, whichinclines to recur after erasure also may metastasize to other places. It befalls due …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 7, Issue 1, 2021 · pp. 51–57 Read article
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Review on Azomethine-Compounds with Their Applications
Abstract: Azomethine derivatives are very important and the initiating compound for most synthetic chemistrycompounds in all their fields. Since R, R1 is an alkyl or aryl group, the first to prepare and isolate itwas the German scientist Hugo Schiff in 1864 from the condensation of the carbonyl group (aldehyde,ketone) with a primary amine compound (aliphatic, aromatic). During the past few decades there hasbeen great interest in Schiff base compounds. The rules …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 7, Issue 2, 2021 · pp. 1–10 Read article
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NBR/PVC Blends Production, Testing and Applications: An Overview
Abstract: PVC due to its polar nature allows preparation of compatible blends with other polymers. Main and unique property of NBR is its oil resistance and it is used in such application even after higher cost than natural and synthetic rubbers. PVC possesses good oil resistance but needs additional plasticizer which can be extracted by solvents; thus, plastic becomes hard and brittle during the life cycle of the product. There are …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 7, Issue 2, 2021 · pp. 22–25 Read article
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SYNTHESIS OF NICOTINE CORE UNIT OF 2-NITRO-3-PHENYLPROPAN-1-OL FROM BAYLIS-HILLMAN ADDUCTS DERIVED FROM NITRO OLEFINS.
Abstract: The Baylis-Hillman adducts derived from nitroolefins have been conveniently transformed into 2- nitro-3-phenylpropan-1-ol via simple reaction condition. These compounds have been demonstrated for the synthesis of reduction olefin is highly biological reactive compounds. This novel nitro derivative of the BH adduct was simply treated with mole percentage of iron and acetic acid in reactive condition. Hence this novel nicotine core unit compounds were very intrusting and new opportunities for the …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 7, Issue 2, 2021 · pp. 26–30 Read article
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Synthesis of Nano-ZnO by Chemical Method and its Characterization
Abstract: Nanocrystals of ZnO were prepared by chemical method using Zn (II) acetate and potassium hydroxide as the starting materials and methanol as solvent. The material was characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), electron diffraction analysis (EDS), UV-Visible spectroscopy, Dynamic light scatteringanalysis (DLS) and Fourier transform spectroscopy (FTIR) techniques. The results indicated that the obtained ZnO material was in nano-dimension and possessed pure …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 8, Issue 1, 2022 · pp. 13–18 Read article
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Eco-friendly Color Production for Holi Celebration: A Mini Review
Abstract: Many synthetic colours formed from chemicals have adverse effects on environment. Biocolours are nowadays used in holi festival. Colours are also becoming integral part of modern day life. Use of colours are becoming a part of our everyday life. There is need of nontoxic colours in order to remove substances like lead, cadmium, chromium and cobalt entering in the food chain. Biocolours are mainly prepared from plant origins. The current …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 8, Issue 1, 2022 · pp. 7–12 Read article
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Experimental Study on Synthesis of Shear Thickening Fluid
Abstract: A novel class of nanosuspension material called shear thickening fluids (STFs) are created by dispersing micro- and nanoparticles in a dispersant. It is an intelligent material with excellent performance. When a modest shear rate is used, STFs are easily distorted. A material with noticeably improved characteristics is produced by this mixture (STF) of flowable and rigid components at a certain composition. Silica nanoparticles dispersed in a liquid polymer solution were …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 8, Issue 2, 2022 · pp. 1–6 Read article
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Achieving Energy Economy and Sustainable Development by Decentralized Energy Planning in Angkuchen Village, Sikkim A Case Study
Abstract: Energy is the fuel for the growth of human civilization. But what becomes of utmost importance by current trends is proper management of the energy resources. The commercial energy consumption, in current state of affairs, is about 67% of the total energy consumed in India. This includes coal with the largest share of 57%, followed by oil at 28%, natural gas at 12% and hydro energy at 3%. Non-commercial energy …
Published in International Journal of Renewable Energy and its Commercialization · Vol. 1, Issue 1, 2015 · pp. 6–12 Read article
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An overview of current activities in commercial deployment of hydrogen energy projects around the world
Abstract: Hydrogen energy systems have been proposed as one of the major components of a decarbonized, clean and sustainable energy system of the future, which will also include renewables, nuclear energy and biomass energy forms. Hydrogen production, storage, distribution and re-conversion technologies are essential components of this value chain. This study looks at some commercial level technologies available and projects deployed round the world for ushering in hydrogen energy systems on …
Published in International Journal of Renewable Energy and its Commercialization · Vol. 6, Issue 2, 2020 · pp. 16–25 Read article
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Review on Production of Activated Carbon from Agricultural Biomass Waste
Abstract: Agricultural biomass waste is one of the main residue largely generated in the environment and was used as precursor for the synthesis of activated carbon as adsorbents, support on catalyst, electric charge storage, micro pore structure, high adsorption capacity material. Recently, many research paper can be found on particular biomass feedstock and activation technique to produce activated carbon. Consequently, main focus should be taken to the relevance those precursor effectiveness …
Published in International Journal of Renewable Energy and its Commercialization · Vol. 7, Issue 2, 2021 · pp. 26–37 Read article
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Surface-Driven Capillary Flow of Dyed Ethanol in a Single SU-8 based Microchannel Bend Fabricated on Glass
Abstract: In this experimental work, a single SU-8 based microchannel bend is fabricated on glass by maskless lithography and indirect bonding technique. Dyed ethanol is prepared as working liquid by mixing commercially available food dye with ethanol. Surface-driven capillary flow of dyed ethanol in streamline motion is recorded by a CMOS camera catching 25 frames per second with a corresponding time-scale resolution of 0.04 second. Effect of centrifugal force on surface-driven …
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 6, Issue 1, 2020 · pp. 29–34 Read article
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Thermodynamic Explanation on Surface-Driven Capillary Flow of Working Liquids in the Microfluidic Devices Fabricated by Polymers
Abstract: In this experimental work, total 100 individual microfluidic devices are fabricated by polymers using author’s own hands-on completely. A set of straight microchannels, gradual expansion microchannels, sudden expansion microchannels and sudden contraction microchannels are fabricated by SU-8 using the maskless lithography and indirect bonding technique. Another set of straight microchannels, gradual expansion microchannels, sudden expansion microchannels and sudden contraction microchannels are fabricated by PMMA using the maskless lithography, hot embossing …
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 6, Issue 1, 2020 · pp. 45–70 Read article
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Oxidative Desulfurization of Petroleum
Abstract: One of the most successful desulfurization procedures for the creation of ultra-low sulphur import fuels is oxidative desulfurization, which converts aromatic sulfur-containing molecules into sulfone counterparts before being extracted. Oxidative desulfurization processes using graphene oxide are of great interest for fuel sulfur removal. Its technique of desulfurization in reactions catalyzed was thoroughly detailed in this review, along with graphene’s function as a supported catalyst, the findings of research on oxidative …
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 8, Issue 2, 2022 · pp. 1–4 Read article
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Study on the Effects of Polypropylene Fiber in Concrete Paver Blocks
Abstract: Road transportation is the lifeline of the nation and its development is a crucial concern. The traditional bituminous pavement needs the continuous maintenance and rehabilitation operations, which ultimately leads to the scope for cement concrete pavements. This paper highlights the effects of polypropylene fibers in concrete paver blocks, which is a recent advancement in the field of reinforced concrete pavement design. Concrete paver blocks prepared for M30 grade and the …
Published in International Journal of Construction Engineering and Planning · Vol. 3, Issue 2, 2017 · pp. 32–38 Read article
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Compressive Strength, Water Absorption and Temperature Effects on Partial Replacing Cement with GGBS, Micro Silica and Fly Ash
Abstract: Widespread research work for decades also in development throughout the globe in concrete technology in finding substitute materials which can incompletely change Pozzolonic Portland Cement (PPC) and which can also meet the necessities of the strength and durability performance of industrial by products like micro silica, ground granulated blast furnace slag, fly ash, etc. now termed as complimentary cementations materials (CCM) are quite promising. The increased quest for sustainable and …
Published in International Journal of Construction Engineering and Planning · Vol. 4, Issue 2, 2018 · pp. 30–37 Read article
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Strain-based Fatigue Test of Woven Glass-Epoxy Fabric Composites
Abstract: Strain based fatigue testing of Glass-Epoxy Composite Material in Tension-Tension loading is carried out by using positive load method to evaluate potential crack propagation, fiber fractures, de-laminations, etc. Through continuous stressing in the material, evaluation of life cycle capabilities of glass fiber composites are found which is essential for Research Development, Structural Design, Quality assurance, Modeling and finally Material Specifications. By using an epoxy resin with glass fiber prepared in …
Published in International Journal of Construction Engineering and Planning · Vol. 5, Issue 1, 2019 · pp. 39–55 Read article
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Analysis of Critical Success Factors for Metro Construction Projects in India
Abstract: Critical success factors pertain to the objectives, principles, and economical performance of theproject. To understand goals and which methods are accustomed to achieve them and also the way tomake efficient its output, these all support designed critical success factor. It is well-known that theconstruction management or industries having dynamic nature due to its everywhere disseminationthrough technologies and within the developing countries, the construction industry is one altogetherthe foremost job creators. …
Published in International Journal of Construction Engineering and Planning · Vol. 7, Issue 1, 2021 · pp. 1–5 Read article