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356 articles for “SEM”
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Induced codeposition of Ni-W alloy coatings using glycerol as additive and their characterization
Abstract: As a promising coating material to replace hard chromium coating, the development of nickel–tungsten (Ni-W) alloy coatings of good corrosion protection is of great interest in surface coating technology. Further, the effect of plating variables, including additive on the composition of alloys of induced co-deposition is more vagarious than in other types of alloy deposition. In this regard, an alkaline citrate bath has been formulated for electrodeposition of Ni-W alloy …
Published in International Journal of Chemical Engineering and Processing · Vol. 2, Issue 2, 2016 · pp. 1–9 Read article
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Electrolytic Deposition of Zn–Ni Alloy from Acidic Sulphate Bath and Their Characterization
Abstract: A bath containing ZnSO4.7H2O, NiSO4.7H2O, thiamine hydrochloride (THC) and citric acid (CA) has been proposed. Bright Zn–Ni alloy coatings were developed galvanostatically onto mild steel (MS) and their corrosion resistance and other physical properties were studied. THC was found to improve the brightness and homogeneity of the deposit. The dependency of bath composition, current density (c.d.), pH and temperature, agitation on wt.% Ni were tested. Deposition was carried out under …
Published in International Journal of Chemical Engineering and Processing · Vol. 2, Issue 2, 2016 · pp. 19–32 Read article
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A Study on the Effect of Current Density on Electrocatalytic Behavior of Ni–Co Alloy
Abstract: Active, stable and more efficient electrocatalysts are the requirements for water splitting applications. In this direction, the present paper presents the experimental results on electrolytic development of Ni–Co alloy coatings, and their application as electrode material for hydrogen evolution reactions (HER) and oxygen evolution reactions (OER). The Ni–Co alloy coatings were electrodeposited on copper substrate from a sulfate bath, using the glycerol as additive. The deposited coatings were then tested …
Published in International Journal of Chemical Engineering and Processing · Vol. 3, Issue 1, 2017 · pp. 9–23 Read article
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Production of Compositionally Modulated Nanolayer Zn–Ni Alloy Coatings and Their Corrosion Behaviours
Abstract: Compositionally modulated nanolayer alloy (CNA) coatings of Zn–Ni having alternatively the same compositions have been developed galvanostatically on mild steel from single bath technique (SBT) using square current pulses. Sulphanilic acid and citric acid (CA) were used as additives. Modulation in the composition of alloys were introduced by passing a different switched cathode current densities (SCCD’S) using sophisticated power sources. Variety of CNA coatings was developed under different conditions of …
Published in International Journal of Chemical Engineering and Processing · Vol. 3, Issue 1, 2017 · pp. 1–8 Read article
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Biosensor –The Future of Diagnostic Study
Abstract: Electrochemical sensors for several analytes were the first technically proven as well as commersialised biosensors. Electrochemical biosensors have been considered for a long time. Presently, typical platform of transducers based on semiconductors and screen printed electrodes is in practice for construction of biosensors. Among all biocomponents, enzymes or enzyme labeled antibodies are presently the most widely recognized biorecognition devices utilized as a part of biosensor. This article focuses the principle …
Published in International Journal of Chemical Engineering and Processing · Vol. 3, Issue 1, 2017 · pp. 36–40 Read article
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Influences of Layered Silicate Modification and Compatibilizers on the Properties of Polypropylene Nanocomposites
Abstract: In this study, polypropylene (PP) organo-layered silicate nanocomposites based on organo-muscovite (OM) were fabricated using co-rotating twin-screw extruder. Polypropylene grafted maleic anhydride (PPMA) and potassium succinate modified polypropylene grafted maleic anhydride (PPKS) were used as a compatibilizer in the nanocomposite system. The influences of layered silicate modification and compatibilizers on the morphological, mechanical, thermal and rheological features of PP/PPMA/OM and PP/PPKS/OM nanocomposites were examined. TEM micrographs were made which showed …
Published in International Journal of Chemical Engineering and Processing · Vol. 7, Issue 1, 2021 · pp. 36–44 Read article
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Physico-Mechanical Performance of Waste Plant Fiber Reinforced Thermoplastic Composites for Automotive Applications
Abstract: To maximize the interfacial bond strength, it is necessary to investigate the direct relationship between the degree of fiber-matrix adhesion and the mechanical and fracture behavior of composites. In this work, the strength of the interfacial bond between polypropylene (PP) and waste plant fiber (Dharose plant fiber, DF) that have been subjected to ultraviolet radiation (UV) was established. By using hot press molding, unidirectional composites of PP with dharose plant …
Published in International Journal of Chemical Engineering and Processing · Vol. 9, Issue 1, 2023 · pp. 14–24 Read article
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Bioethanol Production from Corncob Cellulosic Biomass: RSM and ANN based Optimization for Dilute Acid Pretreatment
Abstract: To increase the yield of fermentable sugars, the complexity of lignocellulosic biomass requires a pretreatment method. Dilute acid hydrolysis was used to efficiently pretreatment corn cobs. The aim of this study was to characterize corncob and investigate the effect of process parameters on total reducing sugar (TRS) yield during dilute acid hydrolysis pretreatment of corncob biomass. The morphology and microstructure of the samples were examined using an X-ray diffraction machine, …
Published in International Journal of Chemical Engineering and Processing · Vol. 9, Issue 2, 2023 · pp. 16–34 Read article
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Pyrolysis Characteristics and Isoconversional kinetics of kusum deoiled seedcake.
Abstract: The pyrolysis characteristics and kinetics of kusum de-oiled seed cake were conducted using a Thermo gravimetric analyzer. Thermogravimetric analysis of biomass was carried out at three different heating rates of 10, 20, 30, ̊ C/min from 28 ̊ C to 1000 ̊ C under N2 atmosphere. The results indicated that the biomass was decomposed in the temperature range of 270 ̊C to 520 ̊ C and further decreased when temperature …
Published in International Journal of Environmental Chemistry · Vol. 2, Issue 2, 2016 · pp. 9–17 Read article
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Preparation and Characterization of Ce-Si-SBA-15 Modified With Iron
Abstract: Recently environmental concerns have driven the development of specialized catalysts to prevent polluting substances from being released into the environment. New technologies have improvised our understanding of catalytic functions as well as selectivity in order to save the energy and chemicals. Today, catalysis is the workhorse in the chemical industry with approximately >90% of the products produced in catalytic processes. In addition, life cannot exist without catalysis, as virtually all …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 2, Issue 1, 2016 Read article
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Studies on Zirconium(IV) Telluroiodate: A New Heteropolyacid Based Inorganic Ion Exchange Material
Abstract: Zirconium (IV) telluroiodate has been synthesized as a new inorganic cation exchanger by adding a mixture of aqueous solution of 0.1 M potassium iodate and 0.1 M sodium tellurite to aqueous solution of 0.1 M zirconium (IV) oxychloride under varying mixing ratios at pH 1. Its ion exchange capacity for Na+ was found to be 1.85 meqg1 of dry exchanger. The material has been characterized on the basis of chemical …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 2, Issue 1, 2016 Read article
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Preparation and Evaluation of Nano pore Faujasite Membranes
Abstract: Nano pore Faujasite zeolite membranes were synthesized by in-situ hydrothermal method on porous ceramic tubes. Hydrothermal crystallization was carried out under an autogenously pressure and at a static condition of 100 oC. Molar composition of the starting gel of Faujasite zeolite membranes were NaX: SiO2/Al2O3=10-27, Na2O/Al2O3=4-9, H2O/Al2O3=250; NaY: SiO2/Al2O3=2.5-4, Na2O/SiO2=1.08-2, H2O/Na2O=30-200. X-ray diffraction (XRD) patterns of the membranes exhibited peaks corresponding to the support and the zeolite. The crystal species …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 3, Issue 2, 2017 · pp. 15–24 Read article
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REVIEW ON PREPARATION & APPLICATIONS OF THIADIAZOLE DERIVATIVES
Abstract: This review has touched on thiadiazole derivatives as it is a basis for the synthesis of many drugs, industrial compounds, chemical dyes, pharmaceuticals and life substances, and as a link to many cyclic reactions and is produced in vitro methods for the hydrolysis of the amine-thiol compounds such as thiosemicarbazide and hydrazo-thion, among others. On the different methods of preparation for thiadiazole derivatives, its reactions and its various biological applications., …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 6, Issue 1, 2020 · pp. 19–30 Read article
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REVIEW ON PREPARATION METHODS & APPLICATION FIELDS OF OXADIAZOLE
Abstract: This review displays oxadiazole (five-ring) that is of great importance in the fields of pharmacy, medicine, and field of coordinated chemistry and as reagents to estimate the small quantities of trace elements and minerals. Oxadiazole is a primary role and as a basic substance for many pharmacokinetic compounds such as antimalarial drugs, anti- bacterial, and cancerous tumors. This survey described several approach for preparation methods of oxadizole with their applications …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 6, Issue 1, 2020 · pp. 49–60 Read article
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Synthesis of Nano-ZnO by Chemical Method and its Characterization
Abstract: Nanocrystals of ZnO were prepared by chemical method using Zn (II) acetate and potassium hydroxide as the starting materials and methanol as solvent. The material was characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), electron diffraction analysis (EDS), UV-Visible spectroscopy, Dynamic light scatteringanalysis (DLS) and Fourier transform spectroscopy (FTIR) techniques. The results indicated that the obtained ZnO material was in nano-dimension and possessed pure …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 8, Issue 1, 2022 · pp. 13–18 Read article
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Green Chemistry Approach for the Preparation of Silver Nanoparticles: A Review
Abstract: The word "nanoparticles" refers to particles within a size range of 10 and 100 nm. Nanotechnology is the topic that is growing the fastest because of its applications in science and technology to produce new at the nanoscale range. Silver is the metal of first preference among the various noble metals. The production of silver nanoparticles can be achieved by different methods such as: chemical method, biological method, green synthesis. …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 9, Issue 1, 2023 · pp. 30–39 Read article
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Magnesium Doped Ammonium Di Hydrogen Phosphate
Abstract: New mixed crystals of Ammonium magnesium sulphate heptahydrate (AMgS) are synthesized by slow evaporation solution growth process using water as solvent. Close observation of FTIR and XRD profiles of doped and undoped samples reveal some minor structural variations. Energy dispersive spectra shows the presence of Mg (II) in the doped crystals. The sample's purity is verified through thermal analyses. SEM images exhibit defect centers due to dopants incorporation into ADP …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 9, Issue 1, 2023 · pp. 40–52 Read article
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Synthesis, Crystal growth and Characterization of Lead acetate zinc (II)Sulphate Material
Abstract: Leadacetatezinc (II) Sulphate Crystal is synthesized by the addition of Leadacetate to Zinc sulphate in equimolar concentration (1:1ratio) to produce larger sized crystal but during the crystallization process a bulk of colourless precipitate was obtained and after filtration the crystals are formed in the filtrate after slow evaporation solution growth technique. Thus formed crystals from the filtrate is kept away and the precipitate formed during the crystallization process is characterized …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 9, Issue 1, 2023 · pp. 22–29 Read article
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Stability Analysis of Mahua Seed and Waste Polystyrene Co-pyrolytic Oil
Abstract: Biomass pyrolytic oil is a complex mixture of organic compounds and obtained in a non-equilibrium state. Hence, the physical properties of bio-oil such as calorific value, viscosity, pH, density, flow ability and chemical compositions vary during storage. In this study, co-pyrolysis of Mahua seed was performed with waste polystyrene and studied the fuel properties and composition. The co-pyrolytic oil was produced at 2:1 ratio of seed to waste polystyrene using …
Published in International Journal of Renewable Energy and its Commercialization · Vol. 2, Issue 1, 2016 · pp. 1–7 Read article
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Studies on the Kinetics of Thermal Decomposition of Copper Oxalate Mixed With Silver Oxalate
Abstract: The coprecipitates, Ag2Cu(C2O4)nH2O of varying composition [Ag = (1 and 2)%], have been synthesized and were characterized by means of IR, XRD, and SEM. The decomposition of the prepared oxalates was monitored by differential scanning calorimetry (DSC) and thermogravimetry (TG). The DSC studies reveal that the decompositions of the mixed oxalates were all complex exothermic processes with resemblance to the exothermic reaction of copper oxalate and ranges from 540 to …
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 2, Issue 1, 2016 · pp. 1–11 Read article