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SYNTHESIS AND CHARACTERIZATION OF MIXED LIGAND COMPLEXES OF HYDROXAMIC ACIDS WITH POTASSIUM HEXATHIOCYANATO CHROMIUM (III) TETRA HYDRATE
Abstract: Some hydroxamic acids eg.[L1= benzohydroxamic acids (BHA), L2= N-phenyl– benzohydroxamic acid (NPBHA), L3= pivaloyl benzohydroxamic acid (PHA) and L4=N-phenyl-pivaloyl benzohydroxamic acid (PPHA) prepared and reacted with L’=Potassium hexathiocynato chromium (III) tetra hydrate K3[Cr(SCN)6]4H2O.The mixed ligand complexes of hydroxamic acids characterized with the help of repeated melting point, by I.R. studies, magnetic moment, molar conductance and by elemental analysis(C,H and N).The stoichiometry of the complexes were found to be 1:2(M:L) molar …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 2, Issue 2, 2016 Read article
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Preparation and Evaluation of Nano pore Faujasite Membranes
Abstract: Nano pore Faujasite zeolite membranes were synthesized by in-situ hydrothermal method on porous ceramic tubes. Hydrothermal crystallization was carried out under an autogenously pressure and at a static condition of 100 oC. Molar composition of the starting gel of Faujasite zeolite membranes were NaX: SiO2/Al2O3=10-27, Na2O/Al2O3=4-9, H2O/Al2O3=250; NaY: SiO2/Al2O3=2.5-4, Na2O/SiO2=1.08-2, H2O/Na2O=30-200. X-ray diffraction (XRD) patterns of the membranes exhibited peaks corresponding to the support and the zeolite. The crystal species …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 3, Issue 2, 2017 · pp. 15–24 Read article
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Different type of catalysts used in the Baylis-Hillman reaction
Abstract: The Baylis-Hillman reaction in the present-day version is an atom-economic carbon-carbon bond-forming reaction between the α-position of the activated alkenes and carbon electrophiles under the influence of a catalyst or catalytic system offering diverse classes of densely functionalized molecules. If the substrate contains both the activated alkene and electrophile components in appropriate positions, there is the possibility of developing an intramolecular version of this reaction leading to the synthesis of …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 5, Issue 2, 2019 · pp. 30–37 Read article
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Magnification of the Mechanism of Enzyme Catalyzed Reaction through Geometric Model
Abstract: The geometric model is dealing with correlation between the “five events for enzyme catalyzed reaction” and “triple point event serving groups on the circle” in triangle obtained for thegraphical presentation of the double reciprocal (1÷S versus 1÷V) for magnification of the mechanism of enzyme catalyzed reaction. This model is based on the nine point circle in triangle of the double reciprocal plot. The five significant points resulted for the circle …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 6, Issue 2, 2020 · pp. 1–25 Read article
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Design of a Continuous Stirred Tank Reactor for Acetic Acid Production Using Homogeneous Catalyzed Reaction
Abstract: The carbonylation of methanol to give acetic acid is one of the most important homogeneously catalyzed industrial processes. Detailed work has been carried out by researchers on its kinetic study and attempt to increase the activity of the catalyst. In this work attention is focused on the design of a continuous stirred tank reactor (CSTR) for the production of 210, 000 tons per year of acetic acid. At a maximum …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 7, Issue 1, 2021 · pp. 17–38 Read article
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Extraction of Xylanases from Media Based on three Agricolous Co-products by An Aqueous Two-phase System
Abstract: Jonesia denitrificans BN13 grows very well on a medium made out of agricultural byproducts like orange peel, esparto grass, and retam; the relative enzyme activity of these three substrates was 0.662, 0.711, and 0.835 U/ml, respectively First time xylanases were effectively extracted utilising aqueous two-phase system (ATPS) that had 3.5% PEG, 14% KH2PO4/K2HPO4, and 9% KI, The inclusion of cells resulted in much improved output from the system, which is …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 8, Issue 2, 2022 · pp. 7–15 Read article
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Production and Characterization of Biomass Briquette from Sawdust and Cow Dung Admixture for Domestic Cooking Applications in Northern Ethiopia
Abstract: This study explored the possibility of producing and characterize biomass briquettes from sawdust and caw dung admixture that could be used as a sustainable fuel sources of energy supply for domestic cooking applications. In this study, Potato starch used as a binder. The physical and composition properties of the sawdust and cow dung as well as the developed biomass Briquettes were determined using Thermogravimetric analysis. A portion of sawdust and …
Published in International Journal of Renewable Energy and its Commercialization · Vol. 5, Issue 2, 2019 · pp. 49–57 Read article
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INVESTIGATION ON PORTABILITY OF OTUOKE UNDERGROUND WATER.
Abstract: The study was designed to investigate the portability on groundwater in Otuoke, Bayelsa State. A total of four groundwater samples were acquired and analyzed for their physico-chemical and heavy metal parameters. Heavy metals were all analyzed with the Atomic Absorption Spectrometer and spectrophotometer. The result revealed that for the heavy metals, iron was most predominant, ranging from 0.70 to 0.08 mg/L. Arsenic was below the machine detectable limit and Assessment …
Published in International Journal of Renewable Energy and its Commercialization · Vol. 8, Issue 2, 2022 · pp. 30–36 Read article
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Determination of the optimum magnetic exposure time for magnetic water concrete
Abstract: The purpose of this study was to investigate the effect of magnetic water on the workability and compressive strength of concrete, and also to find the optimum time for exposing water to magnetic field, for which maximum compressive strength of concrete will be achieved. In this research, water was exposed to magnetic field of 336mT per magnet for a duration of 12, 18, 24, 36, and 96 hours, after which …
Published in International Journal of Construction Engineering and Planning · Vol. 6, Issue 1, 2020 · pp. 34–42 Read article
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Innovative Concrete Composites: Assessing Mechanical Strength with Fly Ash, Glass, and Granite Waste Incorporation
Abstract: Waste management poses a significant challenge for countries in both current and future contexts. The generation of solid waste from various industries, such as stone, glass, coal, and tires, constitutes a major issue in India, leading to significant environmental and health concerns for the surrounding population. This study addresses these challenges by exploring the utilization of waste granite and glass powder as materials to replace sand and cement, respectively, with …
Published in International Journal of Construction Engineering and Planning · Vol. 9, Issue 2, 2023 · pp. 37–45 Read article
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INVESTIGATION OF STEEL FIBER REINFORCED CONCRETE CORBELS BY EXPERIMENTAL AND ANALYTICAL METHOD
Abstract: In the present paper, an experimental results and predicted values by truss analogy method, ACI Building Code (ACI 381-83) provisions for corbels, and method given by Fattuhi is investigated. The concrete used in the corbels is of M-60 grade. Test were carried out on 27 samples of size 150 x 150 x 200- mm were shear span was varied from 175 to 200 as shown in table (5) and concrete …
Published in International Journal of Concrete Technology · Vol. 2, Issue 2, 2016 · pp. 23–29 Read article
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Effect on Strength Properties Concrete Amalgamation of Recycled Reinforced Aggregate -An Experimental Study
Abstract: Concrete is a combination substance which has turn into a universal and essential as its intrinsic in character brought an uprising application. Use of concrete in construction lead to construction of surplus desecrate subsequent to destruction of the variety of structures. The waste generated is enormous and uncontrollable. So, in this present research is to verify the potency of concrete with normal aggregate and recycled aggregate in addition to enlarged …
Published in International Journal of Concrete Technology · Vol. 6, Issue 1, 2020 · pp. 7–15 Read article
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Impact of Additives on the Split Tensile Strength of Roller Compacted Concrete
Abstract: Additives are implemented as partial replacement of Portland cement in concrete to enhance the required physical properties. In the present investigation, roller compacted concrete slab samples were prepared using gap and dense aggregate gradation. Three percentages of Portland cement were adopted, (16, 12, and 10) % by weight of aggregates. Three types of additives, (hydrated lime, fly ash, and fumed silica) were implemented as partial substitute of Portland cement. Core …
Published in International Journal of Concrete Technology · Vol. 7, Issue 2, 2021 · pp. 9–15 Read article
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Application of Suitable Admixtures (Lime and RHA) for Improvement of Pavement Subgrade
Abstract: Abstract The quality of a pavement depends on the strength of its sub-grade. The present investigation has been carried out with easily available materials like lime and rice husk ash mixed individually and in combinations with different proportions. The different percentages of lime with respect to weight of dry soil were 2%, 4%, 6%, 8% 10% and for rice husk ash (RHA) were 3%, 6%, 9% and 12%. In each …
Published in International Journal of Geological and Geotechnical Engineering · Vol. 1, Issue 2, 2015 · pp. 14–31 Read article
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A Review of Geophysical, Geochemical and Geotechnical Study of the Marine Soil of Mahakalapada With Special Allusion to Its Stratigraphic Set-up
Abstract: The present study deals with the marine soil properties collected from Mahakalapada of Kendrapara district in Odisha. Five numbers of saturated soil samples were collected from 2ʹ to 3ʹ below the earth surface and were mixed thoroughly to get the best result. The soil was initially air dried in open atmosphere prior to the testing. The various properties of each sample was calculated either in-situ or in the laboratory. The …
Published in International Journal of Geological and Geotechnical Engineering · Vol. 3, Issue 2, 2017 · pp. 16–23 Read article
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Seismic Hazard Assessment of Dehradun City
Abstract: Seismic hazard assessment refers to an estimation of ground motion parameters at any site or region. In the present study seismic hazard assessment is performed for the Dehradun city which lies in a highly seismic region in the Himalayan foothills. Based on the seismicity data provided by IMD, New Delhi and Seismotectonic Atlas of India (GSI, 2000), seismicity was described and 24 seismotectonic sources were identified in the study area. …
Published in International Journal of Geological and Geotechnical Engineering · Vol. 4, Issue 1, 2018 · pp. 6–12 Read article
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Simplified Analytical and Numerical Analysis for Stability of Tunnel and Foundation Containing Sloping Ground
Abstract: Tunnel, foundation and superstructure effect on the stability of slope. Numerical and simplified analytical analyses evaluate behavior of slope under various conditions. However, factor of safety indicates failure criteria of slope. Present research develops some simplified analytical formulae for a specific model and numerical code (PLAXIS 3D) performs finite element analysis of this model. During numerical analysis considers Mohr-Coulomb material model and drained condition. Factor of safety assesses from variations …
Published in International Journal of Geological and Geotechnical Engineering · Vol. 7, Issue 2, 2021 · pp. 24–34 Read article
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Design of Deep Beam Using Strut-and-Tie Method A Case Study of Pile Cap
Abstract: This study takes a look at modeling of deep beam using strut-and-tie method using pile cap as a case study. There are B and D region in the deep beam (B standing for beam or Bernoulli and D standing for discontinuity or disturbance). A deep beam has a span-depth, a/d ratio ranging from 2.0 to 2.5. Thereafter, the strut-and-tie modeling (STM) of pile cap was displayed. The STM was later …
Published in International Journal of Structural Engineering and Analysis · Vol. 4, Issue 1, 2018 · pp. 6–14 Read article
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Influence of Moisture Damage on Resilient Modulus of Asphalt Concrete
Abstract: Deterioration of asphalt concrete pavement by the action of moisture damage is a major problem facing the serviceability and durability of flexible pavement, it starts with micro cracking of the pavement surface due to load repetitions, and followed by stripping and disintegration of pavement layer. In this investigation, the influence of moisture damage on resilient modulus of asphalt concrete had been assessed under repeated tensile and shear stresses. Asphalt concrete …
Published in International Journal of Transportation Engineering and Traffic System · Vol. 2, Issue 2, 2016 · pp. 12–19 Read article
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Flexural Behavior of Recycled Asphalt Concrete
Abstract: The operational health of the road network is of the utmost importance for economic and social life. Fatigue life is affected by the growth and accumulation of cracks, under the action of repeated vehicular loading, aging and effect of the environment. The flexural behavior of asphalt concrete depends mainly on the flexibility of the pavement mixture which deteriorate gradually with time. Recycling could be a suitable action to reserve such …
Published in International Journal of Transportation Engineering and Traffic System · Vol. 4, Issue 2, 2018 · pp. 32–37 Read article