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85 articles for “XRD”
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Synthesis, Crystal growth and Characterization of Lead acetate zinc (II)Sulphate Material
Abstract: Leadacetatezinc (II) Sulphate Crystal is synthesized by the addition of Leadacetate to Zinc sulphate in equimolar concentration (1:1ratio) to produce larger sized crystal but during the crystallization process a bulk of colourless precipitate was obtained and after filtration the crystals are formed in the filtrate after slow evaporation solution growth technique. Thus formed crystals from the filtrate is kept away and the precipitate formed during the crystallization process is characterized …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 9, Issue 1, 2023 · pp. 22–29 Read article
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Catalytic Steam recycle of Bio-Oil Produces Hydrogen
Abstract: The "water-gas shift reaction" is a process that combines the vapour and carbon monoxide to produce carbon dioxide and more hydrogen.Steam reforming of actual bio-oil is a more realisticmethod for producing H2 despite substantial research on the heat reform of model compounds (such as ethanol). With a focus on the creation of catalysts for the procedure, this paper covers current developments in the steam reforming of actual bio-oil. Given its …
Published in International Journal of Renewable Energy and its Commercialization · Vol. 8, Issue 1, 2022 · pp. 25–29 Read article
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Characterization and Kinetic Study of Sugarcane Bagasse for the Production of Bio-oil Over Monodispersed Fe2 O3 and ZSM-5 Composite
Abstract: The shortage and price scramble of fossil fuels accompanied by vast CO2 emissions have triggered a worldwide search for alternative and sustainable resources. Wind, solar, geothermal, biomass, and water are the most commonly used alternative energy sources. The biomass residues are typically at low cost and readily availabile, and has been used as feedstocks for synthesis of renewable energy. To produced the bio-fuels from biomass residues, several reaction pathways categorized …
Published in International Journal of Renewable Energy and its Commercialization · Vol. 9, Issue 2, 2023 · pp. 1–13 Read article
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Studies on the Kinetics of Thermal Decomposition of Copper Oxalate Mixed With Silver Oxalate
Abstract: The coprecipitates, Ag2Cu(C2O4)nH2O of varying composition [Ag = (1 and 2)%], have been synthesized and were characterized by means of IR, XRD, and SEM. The decomposition of the prepared oxalates was monitored by differential scanning calorimetry (DSC) and thermogravimetry (TG). The DSC studies reveal that the decompositions of the mixed oxalates were all complex exothermic processes with resemblance to the exothermic reaction of copper oxalate and ranges from 540 to …
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 2, Issue 1, 2016 · pp. 1–11 Read article
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Fresh and Hardened Properties of High Performance Concrete with Weld Slag as Fine Aggregate
Abstract: This research centers on the incorporation of welding slag, the residue remaining after the welding process, as fine aggregates in the production of high-performance concrete with a compressive strength of 70 MPa. The chemical and physical characteristics of welding slag aggregates (WSA), such as chemical compositions, specific gravity, SEM images, XRD, and EDS analysis, were investigated. Additional investigations were carried out by substituting welding slag with standard sand at varying …
Published in International Journal of Construction Engineering and Planning · Vol. 9, Issue 2, 2023 · pp. 29–36 Read article
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Deposition and Characterization of ZnO Thin Films by Thermal Vacuum Thermal Evaporation Method for Photoconductive Sensor Application
Abstract: In this work we have deposited ZnO thin films using thermal evaporation method. The films have been deposited on silicon substrate for structural characterization and on glass substrate for optical characterization. The structural, surface morphology, optical properties and electrical properties of ZnO thin films were investigated systematically using X-ray diffractometer (XRD), scanning electron microscope (SEM), atomic force microscopy (AFM), ellipsometeric measurement and semiconductor parameter analyzer respectively. The deposited ZnO thin …
Published in International Journal of Microelectronics and Digital integrated circuits · Vol. 2, Issue 1, 2016 · pp. 1–7 Read article
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Synthesis of Zinc Oxide Nanoparticles by Simple Hydrothermal Process
Abstract: Rapid synthesis of zinc oxide nanoparticles through economically feasible hydrothermal approach is highly desirable. In this study, we have developed a method to synthesize zinc oxide nanoparticles by using simple hydrothermal process in aqueous zinc salt solution (ZnCl2) without need of any surfactant or external energy. This experimentation produced physiologically stable, bio-compatible ZnONPs which may be used for targeted drug delivery that offers enhanced therapeutic efficacy and minimal side effects. …
Published in International Journal of Applied Nanotechnology · Vol. 2, Issue 1, 2016 · pp. 8–16 Read article
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Synthesis and Characterization of Magnetite-Pectin-Alginate Hybrid and Bionanocomposite
Abstract: It is a one pot synthesis of hybrid bionanocomposite comprising of inorganic magnetite with stabilizer biopolymer pectin and alginate in co-precipitation method using sodium hydroxide and ammonium hydroxide as precipitating agents. A lot of comparison and investigation has been done in particle size of nanocomposite by changing the stoichiometric ratio of both magnetite and biopolymer concentration and drying condition of composite. The nanocomposite has been characterized using infrared spectroscopy (FTIR), …
Published in International Journal of Applied Nanotechnology · Vol. 3, Issue 1, 2017 · pp. 18–22 Read article
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Zinc oxide/Chitosan biocompatible nanocomposites: Preparation, Characterization and its use in Congo red dye photodegradation
Abstract: Zinc oxide/chitosan biocompatible nanocomposites have been successfully synthesized by co-precipitation method. The samples were characterized by X-ray diffraction (XRD), Scanning electron microscope (SEM), Energy dispersive X ray Flurescence spectroscopy (EDAX) and Fourier transformation infrared spectroscopy (FTIR). The photocatalytic efficiency and photostability of the sample was investigated systematically for Congo red degradation under solar light irradiation. UV-vis Spectroscopy was employed to investigate the optical properties and photocatalysis behavior of the Zinc …
Published in International Journal of Applied Nanotechnology · Vol. 3, Issue 2, 2017 · pp. 27–39 Read article
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Synthesis of Silver Nano Particles Using NaBH4 as Reducing Agent
Abstract: Silver nanoparticles (AgNPs) are one of the most vital and captivating nanomaterials between numerous metallic nanoparticles that are involved in various applications. In this paper, we briefly discuss the synthesis of AgNPs properties and application for the nanoparticles. The present work shows that the reduction of silver ions from AgNO3 to Ag occurs due reducing agent. The synthesized silver particles have been characterized by UV – Visible, TEM and XRD …
Published in International Journal of Applied Nanotechnology · Vol. 5, Issue 1, 2019 · pp. 27–33 Read article
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Impact of Substrate Temperature on Chemically Deposited Cds Thin Films
Abstract: The interest for renewable energy sources are increasing day by day due to the limited availability of fossil fuel. Among all the renewable energy sources solar energy is growing interest due to its easy availability almost among all area of earth where people lives. Solar energy can be used as a source of energy by two ways: Solar Photovoltaic Cell and Solar thermal. Photovoltaic cells are the easiest way for …
Published in International Journal of Energetic Materials · Vol. 1, Issue 1, 2015 · pp. 22–26 Read article
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Effect of Sulphamic acid on the growth of Glycine single crystals
Abstract: Sulphamic acid added glycine single crystals were grown successfully by slow-evaporation technique.A single crystal with well defined crystal was obtained. The lattice parameters and crystal system of the grown crystals were confirmed by single crystal and powder x-ray diffraction analysis.The functional groups present in the sample were identified by FTIR spectral analysis.The lower cut off wavelength and bandgap energy of the grown crystal was analysed from uv-vis spectral analysis. Keywords: …
Published in International Journal of Energetic Materials · Vol. 5, Issue 1, 2019 · pp. 9–13 Read article
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Effect of Ge and Pb Impurities on the Optical Properties of Amorphous (Sb2Se3)90Sn10 Thin Films
Abstract: The as prepared samples of [(Sb2Se3)90Sn10]95 M5 [M = Ge, Pb] chalcogenide system were amorphous as evidenced by X-ray diffraction studies. The optical band gap has been estimated with the help of Taucs relation for the as-deposited [(Sb2Se3)90Sn10]95M5 thin films. It is observed that the optical band gap increase with increase in the Ge and Pb content, which may be due to decrease in the density of defect states. This …
Published in International Journal of Metallurgy and Alloys · Vol. 6, Issue 1, 2020 · pp. 7–14 Read article
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Green synthesis of Copper nanoparticles using Ctenolepis garcini (Burm.f.) C.B Clarke.
Abstract: Copper nanoparticles, due to the excellent physical and chemical properties and low cost of preparation, have been of great interest in wide applications as heat transfer systems, antimicrobial materials, super strong materials, sensors and catalysts. The present study is a novel biological approach for the formation of copper nanoparticles using Ctenolepis garcinii (Burm.f.) C.B Clarke. Copper nitrate was made to reduce with aqueous solution of plant extract. UV-Visible spectrum showed …
Published in International journal of Nanobiotechnology · Vol. 3, Issue 2, 2017 · pp. 1–6 Read article
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Formulation and Characterization of Polyhydroxyalkanoates Copolymer Nanoparticles for Controlled Drug Release
Abstract: The present study was focused on the formulation of polyhydroxyalkanoates copolymer nanoparticles (PHANPs) for in vitro controlled release of the drugs, viz. levofloxacin and amoxicillin. The PHANPs were synthesized by a triple emulsion method and conjugated with amoxicillin and levofloxacin to improve its remedial bioavailability. The PHANPs and drug conjugatedPHANPs were analysed using Scanning Electron Microscopy (SEM), Fourier Transform Infrared (FTIR) spectroscopy and X-Ray Diffraction (XRD). The cell viability % …
Published in International journal of Nanobiotechnology · Vol. 6, Issue 2, 2020 · pp. 1–11 Read article
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Trichoderma Based Synthesis of Silver Oxide Nanoparticles, Their Characterization and Assessment of Antifungal Activity
Abstract: The fungal spore suspension of Trichoderma harzianum was used for the preparation of AgO nanoparticles. T. harzianum spore suspension acts as reducing and stabilizing agent for the fabrication of nanoparticles. The synthesized nanoparticles were characterized by X-ray diffractometry (XRD), scanning electron microscopy (SEM), energy dispersive X-analysis (EDAX) and transmission electron microscopy (TEM). The AgO nanoparticles were circular in shape with average diameter 10-20 nm. The AgO nanoparticles showed promising antifungal …
Published in International journal of Nanobiotechnology · Vol. 7, Issue 2, 2021 · pp. 19–25 Read article
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Low Temperature Chemical Synthesis of Nickel Oxide Microflower and Study of its Optical and Thermal Properties
Abstract: A simple rout for the synthesis of flower like nickel oxide nanostructure has been reported using nickel sulphate and potassium per-sulphate as precursor. Efforts were made to see the effect of persulfate amount on different properties of the materials thus two samples were synthesized with different amount of per-sulphate precursors. The as prepared samples were characterized by x-ray diffraction, field emission scanning and transmission electron microscope, thermal gravimetric and differential …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 4, Issue 2, 2018 · pp. 17–24 Read article
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Effect of nano Aluminum on Thermal Behavior and Ignition Characteristics of Al/KClO4 Thermite Composition
Abstract: Ignition experiments of micron size Al/KClO4 (ALCLO) thermite composition was carried out at high heating rate (40°C/min.) using DTA (differential thermal analysis), and it was observed that no ignition took place up to 700°C. Similarly in case of STA (simultaneous thermal analyzer) experiments, no ignition peaks were found up to 1100°C at 20/min. ALCLO when ignited in a bomb calorimeter for heat of combustion output measurement it produced a large …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 5, Issue 2, 2019 · pp. 9–19 Read article
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Correlation for Photocatalytic Degradation Kinetics of Carboxylic Acids by Electrochemically Synthesized Cd/ZnO Nanoparticles and Study of Antibacterial Behaviour
Abstract: Cd/ZnO nanoparticle has been successfully synthesized by electrochemical method which is simple and inexpensive method. The synthesized Cd/ZnO nanoparticle was used has a catalyst for the photodegradation of Oxalic acid, Chloroacetic acid and Formic acid under various experimental conditions by volumetric method. The Cd/ZnO nanoparticles were characterized by various techniques such as SEM-EDAX, UV-Visible spectroscopy, FTIR-IR spectrum and X-ray diffraction studies. The study of UV-Visible spectroscopy revealed that the Cd/ZnO …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 6, Issue 2, 2020 · pp. 1–16 Read article
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Synthesis of Zero Valent Silver Nanoparticles by Chemical Reduction Method and its Application
Abstract: Chemical synthesis is one of the commonly used method for nanoparticles synthesis. Different chemicals acts as reducing agents which converts chemical precursor into its nano form. There are various chemical methods for the synthesis of zero valent silver nanoparticles. The silver nitrate is commonly used as precursor, sodium borohydride acts as reducing agent while sodium dodecyl sulphate stabilizes the formation of nanoparticles. The formation of silver nanoparticles was characterized by …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 7, Issue 2, 2021 · pp. 8–17 Read article