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122 articles for “Spectroscopy”
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Preparation of a composite Materials from activated carbon and waste plastic for water Treatment
Abstract: Insoluble resins offer several advantages in preparation processes, the chemical, photochemical and thermal mechanical properties of composites are largely affected by matrix properties. The aim of our study was a double aspect, the synthesis of a polymer-based ion exchanger from waste polystyrene and the composite material valorization in water treatment. a series of experiments was made to prepare the sulfonated polystyrene ion exchange resin and the composite material based on …
Published in International Journal of Environmental Chemistry · Vol. 5, Issue 2, 2019 · pp. 38–48 Read article
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Multivariate modeling of mineral water Karachi, Pakistan
Abstract: In last few decades the demand of mineral water has increased and is very important for human life due to shortage of pure and clean water. The mineral water is produced by various companies with different names and brand with approval of the relevant authorities. The present study was carried out for the preconcentration and determination of trace amount of metals (Cd, Cu, Pb, Fe, Mn, Ni, and Zn) from …
Published in International Journal of Environmental Chemistry · Vol. 5, Issue 2, 2019 · pp. 49–59 Read article
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Effect of TiO2 on HER Activity of Electrodeposited Zn–Ni Coatings
Abstract: This paper demonstrates the improved electrocatalytic behavior of Zn–Ni alloy coatings for alkaline hydrogen evolution reaction (HER), due to addition of TiO2 nanoparticles into the bath. Zn–Ni alloy coatings have been electrodeposited galvanostatically on copper, with wide compositional range (2.31–7.91 wt. % of Zn) at different current densities (c.d.) between 2.0 and 5.0 A dm-2. The electrocatalytic behaviors of all coatings have been studied for alkaline HER in 1.0 M …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 3, Issue 1, 2017 Read article
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Green Synthesis of Nickel(II) and Zinc(II) Complexes of Bis(Imine) Schiff base Derived from o-vanilline and m-phenylenediamine.
Abstract: The synthesis of Schiff base ligand derived from aromatic aldehyde (o-vanillin) and m-phenylenediamine via liquid-assisted mechanochemical synthesis (LAG) in the presence of small amount of dimethylformamide were reported. The Schiff base complexes of Ni(II) and Zn(II) were also synthesized mechanochemically and characterized using infra-red spectroscopy, thermogrametric analysis, energy dispersive x-ray analysis, powder x-ray diffraction, UV-Visible analysis, conductivity measurement, magnetic susceptibility measurement and CHN, micro-analysis. Infrared spectral study indicated a strong …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 6, Issue 1, 2020 · pp. 31–43 Read article
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SYNTHESIS AND IR-SPECTROSCOPIC STUDY OF MIXED LIGAND COMPLEX COMPOUNDS OF COPPER (II) FORMAT WITH SOME AMIDES
Abstract: Complex compounds of metals with amides, having biological activity are widely used in agriculture. Complex compounds of copper with organic ligands are physiologically active, participating in the vital processes of living organisms; the formiats have bactericidal and fungicidal properties. For the first time, mixed ligand complex compounds of copper (II) formate with formamide, thiocarbamide, acetamide and carbamide in an aqueous solution were synthesized. Using the methods of IR spectroscopy and …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 6, Issue 2, 2020 · pp. 31–38 Read article
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Green Chemistry Approach for the Preparation of Silver Nanoparticles: A Review
Abstract: The word "nanoparticles" refers to particles within a size range of 10 and 100 nm. Nanotechnology is the topic that is growing the fastest because of its applications in science and technology to produce new at the nanoscale range. Silver is the metal of first preference among the various noble metals. The production of silver nanoparticles can be achieved by different methods such as: chemical method, biological method, green synthesis. …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 9, Issue 1, 2023 · pp. 30–39 Read article
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Advance in the Synthesis of Oxadiazole Based Heterocyclic Compound
Abstract: The five members of the heterocyclic ring 1,3,4-oxadiazole are necessary for the production of strong bioactive molecules. Numerous pharmacological effects, including anti-inflammatory, antibacterial, anticancer, antitubercular, anticonvulsant, anti-HIV, hypoglycemic, and antioxidant qualities, are exhibited by this intriguing class of chemicals. We have created four novel 1,3,4-oxadiazole compounds in the continuing study, which are sourced from the NSAID Ibuprofen. Melting point analysis and TLC were used to verify the compounds' purity. Open …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 9, Issue 2, 2023 · pp. 10–15 Read article
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Characterization and Kinetic Study of Sugarcane Bagasse for the Production of Bio-oil Over Monodispersed Fe2 O3 and ZSM-5 Composite
Abstract: The shortage and price scramble of fossil fuels accompanied by vast CO2 emissions have triggered a worldwide search for alternative and sustainable resources. Wind, solar, geothermal, biomass, and water are the most commonly used alternative energy sources. The biomass residues are typically at low cost and readily availabile, and has been used as feedstocks for synthesis of renewable energy. To produced the bio-fuels from biomass residues, several reaction pathways categorized …
Published in International Journal of Renewable Energy and its Commercialization · Vol. 9, Issue 2, 2023 · pp. 1–13 Read article
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EFFECT OF GLUCOSE ON PHYSICO-CHEMICAL PROPERTIES OF SOME SURFACTANT SOLUTIONS
Abstract: Physico-chemical and thermodynamic studies of some aqueous surfactant solutions were carried out by employing conductance and dye solubilization (UV-Vis absorption spectroscopy) techniques. From the above measurements, critical micelle concentration (CMC) and thermodynamic properties of micellization (ΔGomic , ΔHomic and ΔSomic) have been obtained for an anionic [Sodium dodecyl sulphate (SDS)],a cationic [hexadecyl trimethyl ammonium bromide, (HTAB)] and non ionic (Tween-20) surfactant solutions. Effect of mixing cosolute on CMC and thermodynamics …
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 4, Issue 1, 2018 · pp. 1–22 Read article
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Preparation of Beta Lactam Compounds and Study of Thermodynamically Behavior
Abstract: Several Lactam derivatives have been prepared by condensation reaction of folic acid with (4-chloroacetophenone and 4-hydroxyacetophenone) in ethanol. Then the resultant compounds (1,2) react with another Schiff bases by reacting of 4- bromobenzaldehyde with an amino acid (Phenylalanine, Tryptophan, Tyrosine and Histidine) to give bis-β-lactam rings. The structures of target compounds were characterized by many spectroscopic methods including NMR, FTIR technique and their melting points. The β- lactam derivatives were …
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 5, Issue 2, 2019 · pp. 9–15 Read article
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Laws of Thermodynamics Challenge Greenhouse-Gas and CLIMATE- change Hypotheses
Abstract: The greenhouse-gas hypothesis (GGH), i.e., CO2 is the cause of global warming by ~1K from ~1950-2023, is popularly believed to be established scientific truth. It is generally assumed that heat emissions from global fuel combustion are, by comparison, negligible. An application of the Hess-Gibbs 1st law of thermodynamics, however, shows that the enthalpy (H) output from yearly fossil fuel consumption is seven times greater than the H- increase of hypothetical …
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 9, Issue 1, 2023 · pp. 7–19 Read article
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Research Insight on Everest Contaminated by Toxic Metals
Abstract: The goal of this investigation of the Everest was to look at follow component fixations and altitudinal patterns in soil and snow. Mount Everest was chosen since its remote area and amazing height disengages it from limited contamination sources. Soil tests were gathered from Mount Everest by different specialists and the examples were broke down for Pb, Zn, Cd, Ni, Cr, Co, Cu, As, Mn, Hg, and V utilizing inductively …
Published in International Journal of Geological and Geotechnical Engineering · Vol. 2, Issue 2, 2016 · pp. 21–23 Read article
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Modification of Solar Hot Water Heating System
Abstract: In optoelectronics system, the copper sulfide powder plays an important role as a thin film layer. This paper covers fabrication of Copper sulfide (CuS) Powder and its characterization. The fabricated Copper sulfide powder gives better result as compared to commonly used Copper sulfide (CuS) available in the market. In this experiment, the Copper sulfide powder (CuS) was coated on the tubes as a thin film and measured the outlet water …
Published in International Journal of Water Resources Engineering · Vol. 9, Issue 1, 2023 · pp. 33–39 Read article
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Synthesis and Characterization of Magnetite-Pectin-Alginate Hybrid and Bionanocomposite
Abstract: It is a one pot synthesis of hybrid bionanocomposite comprising of inorganic magnetite with stabilizer biopolymer pectin and alginate in co-precipitation method using sodium hydroxide and ammonium hydroxide as precipitating agents. A lot of comparison and investigation has been done in particle size of nanocomposite by changing the stoichiometric ratio of both magnetite and biopolymer concentration and drying condition of composite. The nanocomposite has been characterized using infrared spectroscopy (FTIR), …
Published in International Journal of Applied Nanotechnology · Vol. 3, Issue 1, 2017 · pp. 18–22 Read article
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Synthesis and Characterization of CdS Nanoparticles for LED Application
Abstract: In the present work we have synthesized the size tuned CdS nanoparticles with chemical routes method. Size of the nanoparticle tuned with varying the addition of an appropriate quantity of capping agent. UV spectroscopy used to study the variation of optical properties with tuning the size of nanoparticle. EMA and TBM techniques are used to analyze size and band gap of the quantum dots.
Published in International Journal of Applied Nanotechnology · Vol. 4, Issue 1, 2018 · pp. 12–18 Read article
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To study the Properties of Bio Synthesized Silver Nanoparticles
Abstract: Recently colloids silver nanoparticles have attained much attention in global nanotechnology market due to valuable application for catalytic, biomedical, electronics and widely as Antimicrobial agents. In the present work author have synthesized and characterized the Colloids silver nanoparticles with three biosynthesis methods and the detail characterization of particle has been done by UV–Visible spectroscopy, AFM, FTIR, and with DLS techniques. Particles formation was conformed from UV spectra of nanoparticles. Size …
Published in International Journal of Applied Nanotechnology · Vol. 4, Issue 1, 2018 · pp. 34–40 Read article
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Synthesis and Characterization of Graphene Nanoplatelets & Graphene Oxide Based Nanofluids With Their Comparative Analysis for Heat Transfer Applications
Abstract: Stability and thermal conductivity are the main features of nanofluids. Higher concentration of nanoparticles become the reason of agglomeration, so a balance equation is required for the preparation of remarkable nanofluids in the application point of view. In the present study, we describe a novel synthesis of graphene Nanoplatelets and graphene oxide based nanofluids with different concentration (0.001,0.003,0.005wt %) with the help of stock solution of 1mg/ml. The Hummer’s method …
Published in International Journal of Applied Nanotechnology · Vol. 4, Issue 2, 2018 · pp. 13–29 Read article
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Electrochemical impendence study of an AL 8088 /SiC Nano composite immersed in 1M Acid chloride Medium
Abstract: Aluminum Nano composite have received considerable attention among researcher and engineering as a prominent choice material for building and construction purposes. The preference of Aluminum Nano composite as replacement for conventional Aluminum alloy is chiefly due excellent strength to weight ratio .However the problem of accelerated corrosion attributed to the reinforcement particle used in the production of Aluminum Nano composite is well documented in the literature and serves as potential …
Published in International Journal of Applied Nanotechnology · Vol. 4, Issue 2, 2018 · pp. 6–12 Read article
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Two-dimensional MoS2 Nanosheets: Preparation and Characterization
Abstract: The amazing properties and useful applications of graphene in the field of sensors, electronics and material science opens a new challenges to other two dimensional semiconductor materials. Specially due to extraordinary electronic, mechanical and optical properties, molybdenum disulfide (MoS2) is attracting huge interest in several applications. Single layer MoS2 with direct band gap shows better semiconductor behavior such as photoluminescence, makes them more acceptable in optoelectronic applications in comparison with …
Published in International Journal of Applied Nanotechnology · Vol. 5, Issue 2, 2019 · pp. 17–25 Read article
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Evaluation of Antimicrobial Activity using Zinc Oxide Nanoparticles
Abstract: The goal of the study was to use common laboratory techniques to create Zinc Oxide nanoparticles in a short amount of time and to check the antibacterial activity of zinc oxide nanoparticles on gram negative and gram positive bacteria. Wet chemical technique was used to make zinc oxide nanoparticles. Activity augmentation for Escherichia coli and Staphylococcus aureus were studied when used in combination with Zinc Oxide Nanoparticles. The Nps are …
Published in International Journal of Applied Nanotechnology · Vol. 7, Issue 1, 2021 · pp. 24–27 Read article