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1992 articles for “Keywords”
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Solid state Acid–Base Reactions of Arylamino Nicotinic Acids: X-ray Crystal Structures of Salts
Abstract: 2-(Phenylamino)nicotinic acid (PNA), 2-(methyl(phenyl)amino)nicotinic acid (MPNA), 2-(p-tolylamino)nicotinic acid (TNA) and 2-(methyl(p-tolyl)amino)nicotinic acid (MTNA) are the ampholites which were synthesized by the coupling of respective aryl amines and 2-chloronicotinic acid in the presence of p-tolylsulfonic acid and pyridine. All these molecules were crystallized in different solvents to obtain intra and intermolecular proton transferred adducts in the solid state. TNA is an only compound which has under gone intra (zwitterion) and intermolecular …
Published in International Journal of Analytical and Applied Chemistry · Vol. 1, Issue 2, 2015 · pp. 1–11 Read article
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Development and Validation of a Reversed-Phase HPLC Method for the Simultaneous Determination of Telmisartan and Its Related Compound B (Positional Isomers) in the Bulk Drug
Abstract: A simple, selective, accurate, precise and linear RP-HPLC method was developed and validation for Simultaneous determination of Telmisartan and its related Compound B 4ʹ-[(1,7-Dimethyl-2'-propyl[2,5'-bi-1H-benzimidazol]-1'-yl)methyl][1,1'-biphenyl]-2-carboxylic acid; 4'-[(1,7'-dimethyl-2'-propyl-1H,1'H-2,5'-bibenzo[d]imidazol-1'-yl)methyl]biphenyl-2-carboxylic acid; was accomplished in the bulk drug and synthesis for drug and a tablet formulation using a Reversed Phase High Performance liquid chromatography method with UV detection separation was achieved on Inertsil ODS-3V column (150 × 4.6 mm, 5 μm) (GL Science) as stationary …
Published in International Journal of Analytical and Applied Chemistry · Vol. 1, Issue 2, 2015 · pp. 12–23 Read article
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Micellization investigations of meristyl alcohol based bis-sulfosuccinate gemini surfactant with anionic and nonionic conventional surfactants
Abstract: Micellization studies have been carried out to investigate the mean aggregation number of aqueous solution of newly synthesized bis-sulfosuccinate gemini surfactant based on meristyl alcohol (BSGSMA1,4) using flexible spacer as methylene chain (CH2)4. The methylene chain was introduced via α,ω-dibromo butane in the reaction. The present study explored the effect of prepared gemini towards the two well recognized conventional surfactants i.e. sodium dodecyl sulphate (SDS) and Triton X 100 in …
Published in International Journal of Analytical and Applied Chemistry · Vol. 2, Issue 1, 2016 · pp. 1–8 Read article
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Guar Gum and Its Graft Copolymers: An Overview
Abstract: Guar gum, a naturally occurring polysaccharide, is being widely used in numerous applications. Guar gum is modified by graft copolymerization to improve upon properties. Grafting is an innovative method to produce a new class of semi synthetic polymeric materials. In grafting, while the original properties of polymer remain intact, some additional and useful properties are incorporated. Natural polymers are available in huge quantities on Earth, since billions of years. Guar …
Published in International Journal of Analytical and Applied Chemistry · Vol. 2, Issue 1, 2016 · pp. 15–22 Read article
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Physico-Chemical Study of Rani Pond Water in Winter Season-2015 of Rewa District, Madhya Pradesh, India
Abstract: This paper presents to physico-chemical study of Rani pond water in winter season-2015 of Rewa district, Madhya Pradesh, India. We are analysed to change in physical and chemical properties of Rani pond water due to season. The variable data of samples are within prescribed limits as suggested by World Health Organisation (WHO), Indian Standard (ISI) and BIS desirable limit for drinking water for drinking purpose. Seasonal variation in physical and …
Published in International Journal of Analytical and Applied Chemistry · Vol. 2, Issue 1, 2016 · pp. 9–14 Read article
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Sensitive Spectrophotometric and Flame Photometric Methods for Determination of Diclofenac Sodium in Pharmaceuticals
Abstract: Diclofenac sodium (DFS) is a non-steroidal anti-inflammatory drug (NSAID). Two new analytical methods have been developed for the assay of DFS in its pure form, tablets and injections. Spectrophotometric method is based on the oxidation of drug with known excess of cerium(IV) and oxidation of methyl orange (MO) by residual oxidant and measurement of absorbance of unreacted MO at 470 nm. Flame photometric method is based on the measurement of …
Published in International Journal of Analytical and Applied Chemistry · Vol. 2, Issue 2, 2016 · pp. 1–10 Read article
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Physico-chemical Analysis of Some Soil Sample around Jaypee Nagar Industrial Area in Postmonsoon Season Session 2012–2013 of Rewa, District MP (India)
Abstract: In the present study, various physico-chemical factors were assessed for the whole year during pre- and postmonsoon season session 2012–2013 to determine the impact cement dust on the soil quality around Jaypee Nagar industrial area. Physico-chemical parameters such as pH, electrical conductivity, organic carbon, phosphorus, potassium, CEC, calcium, magnesium, sulphate, are taken. Most of the samples are within permissible limit. The positive correlation was observed among most of the Physico-Chemical …
Published in International Journal of Analytical and Applied Chemistry · Vol. 2, Issue 2, 2016 · pp. 11–16 Read article
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Stability Indicating Spectrophotometric Methods for the Determination of Enrofloxacin in Pharmaceuticals
Abstract: Enrofloxacin (EFX) is a first fluoroquinolone veterinary antibiotic and used for the treatment of some urinary tract, respiratory tract, and skin infectious diseases in pets and livestock. Three simple, selective and stability indicating UV-spectrophotometric methods have been developed and validated for the assay of EFX in bulk drug and in its dosage forms. The first proposed method (method A) is based on the measurement of the absorbance of EFX in …
Published in International Journal of Analytical and Applied Chemistry · Vol. 2, Issue 2, 2016 · pp. 26–37 Read article
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Electrodeposition of Bright Zn–Co–Fe Alloy Coatings on Mild Steel and Their Characterization
Abstract: Sulphate bath having ZnSO4. 7H2O, CoSO4. 7H2O, FeSO4.7H2O and thiamine hydrochloride (THC) and citric acid (CA) in combination, was optimized for deposition of bright Zn–Co–Fe alloy coating on mild steel. Bath constituents and operating parameters were optimized by Hull cell method, for highest corrosion performance against coating. The effect of current density on deposit characters viz., corrosion resistance, hardness, thickness, CCE were evaluated. Potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) …
Published in International Journal of Analytical and Applied Chemistry · Vol. 2, Issue 2, 2016 · pp. 17–25 Read article
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A New Spectrophotometric Method for the Determination of Psilocin and Psilocybin
Abstract: A rapid new spectrophotometric method is developed for the determination of psilocin and psilocybin using the oxidative coupling reaction with 3-methylbenzthiazolinone-2-hydrazone. The method is precise and accurate. It can be applied to the estimation of psilocin and psilocybin in forensic exhibits. Keywords: 3-methylbenzthiazolinone-2-hydrazone, psilocin, psilocybin, spectrophotometry
Published in International Journal of Analytical and Applied Chemistry · Vol. 3, Issue 1, 2017 · pp. 1–8 Read article
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Spectrophotometric Determination of Salicylates in Urine using 3-Methylbenzthiazolinone – 2 – hydrazone
Abstract: A sensitive (direct or with column partition chromatography) spectrophotometric method for the determination of salicylates in urine using 3 – methylbenzthiazolinone - 2 – hydrazone in the presence of ceric ammonium sulfate as an oxidizing agent is presented. Beer’s law is obeyed in the concentration range of 0 – 1.6 µg ml -1. The method is accurately reproducible and can be applied in the analysis of salicylates in urine. The …
Published in International Journal of Analytical and Applied Chemistry · Vol. 3, Issue 1, 2017 · pp. 14–17 Read article
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A Simplified High-Performance Liquid Chromatographic Method For Determination of Vitamin D3 in Human Serum
Abstract: Diabetes is a metabolic disorder caused by defective insulin secretion, insulin action or both. The two major factors for the development of diabetes are pancreatic beta cell dysfunction and insulin resistance. In type 2 diabetes mellitus, production and release of insulin is unobstructed but due to factors like ageing or obesity, the produced insulin cannot compensate for the increased demand. Measurement of the serum level of 25-hydroxyvitamin D3 is the …
Published in International Journal of Analytical and Applied Chemistry · Vol. 3, Issue 1, 2017 · pp. 9–13 Read article
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Functionalization of Reclaim Rubber: Possible Precursor for Polyblends in Engineering Applications
Abstract: Improvements in mechanical and dynamic properties of a blend can be achieved by surface treatments such as grafting of functional groups on one of the blend components or activation by the application of a coating of a polymer. This paper describes the effect of grafting maleic anhydride on reclaim rubber with varying levels of maleic anhydride (i.e., 2 and 5 phr) on open two roll mills. Investigated cure characteristics and …
Published in International Journal of Analytical and Applied Chemistry · Vol. 3, Issue 1, 2017 · pp. 18–23 Read article
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A Sensitive Spectrophotometric Method for the Determination of Diazepam with MBTH
Abstract: A sensitive, specific spectrophotometric method for the determination of diazepam in bulk drug and formulations has been developed. The diazepam is hydrolyzed to yield 2-Methylamino-5- chlorobenzophenone which is coupled with 3-Methyl benzthiazolinone-2-hydrazone, in the presence of ceric ammonium sulphate as an oxidizing agent, to yield a blue colored solution having an absorbance maximum at 585 nm. It obeys Beer’s law in the concentration range of 0 – 4 µg / …
Published in International Journal of Analytical and Applied Chemistry · Vol. 3, Issue 2, 2017 · pp. 1–8 Read article
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Analytical Application of Radioactive Analysis
Abstract: A radioactive tracer, or radioactive label, is a chemical compound in which one or more atoms have been replaced by a radioisotope so by virtue of its radioactive decay it can be used to explore the mechanism of chemical reactions by tracing the path that the radioisotope follows from reactants to products. Keywords: radioactive tracer, chemical analysis, radioisotopes, atoms and molecules
Published in International Journal of Analytical and Applied Chemistry · Vol. 3, Issue 2, 2017 · pp. 32–35 Read article
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Regression Models to Examine Water Quality Index of Akabuta Stream
Abstract: Research carried out in this article is aimed at establishing mathematical tools, models that be used to monitor and predict water quality index concentration of Akabuta stream. The models developed seemed to be useful in monitoring and predicting water quality index as coefficient of determination of station A. Keywords: akabuta, Akabuta community, regression model, stream, water quality index
Published in International Journal of Analytical and Applied Chemistry · Vol. 3, Issue 2, 2017 · pp. 27–31 Read article
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Removal of fluoride from Ground Water Sample Using Basil Leaves as Adsorbent
Abstract: High Fluoride in Ground water has become one of the most important toxicological and geo-environmental issues. During the last decade, high fluoride concentration resulted in a new disease called “Fluorosis” which has been highlighted throughout the world. Among the water treatment methods available, Adsorption is found to be one of the most effective method for water purification. The Present investigation was carried out to find the suitability of Tulsi leaves …
Published in International Journal of Analytical and Applied Chemistry · Vol. 3, Issue 2, 2017 · pp. 23–26 Read article
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Investigation on Synthesis and Evaluation of Nanopore NaA Zeolite Membranes
Abstract: Effects of synthesis parameters on the membrane structure and performance have been investigated for nanopore NaA zeolite membranes grown onto seeded mullite supports. Molar composition of the starting gel of nano NaA membranes was: SiO2/Al2O3=0.8–3.2, Na2O/Al2O3=1.6–4.6, and H2O/Al2O3=50–200. Also, effects of crystallization time and temperature on the membrane performance were studied. X-ray diffraction (XRD) patterns of the membranes exhibited peaks corresponding to the support and the zeolite. The crystal species …
Published in International Journal of Analytical and Applied Chemistry · Vol. 3, Issue 2, 2017 · pp. 9–22 Read article
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DESIGNING OF A LEAN ASSEMBLY LINE FOR NATIONAL HEATER COMPANY AT AL-RUSAYL
Abstract: Most industrial sectors are concerned with reducing wastes activities; therefore they mostly use Lean manufacturing technology as the best solution to accomplish their aim. These non-added value wastes could be unnecessary motion, inadequate processing, excessive transportation, defects, waiting, unnecessary inventory and overproduction. A survey was implemented on both Rusayl Industry Area Company and National Heater Industries Company L.L.C for this study purpose as those two companies are compatible with this …
Published in International Journal of Analytical and Applied Chemistry · Vol. 4, Issue 1, 2018 · pp. 18–35 Read article
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Computational modeling and experimental investigation of using vibration to mixing and separation of a gas bubbles and a liquid in reduced and microgravity conditions
Abstract: The main purpose of the present research is the computational modeling of the gas bubbles behavior in the vibrating fluid under reduced and microgravity conditions. The manuscript presents the results of work of the developed computer model of the gas bubbles behavior in the vibrating fluid under reduced and microgravity conditions, and the experimental investigation of using vibration to mixing and separation of a gas bubbles and a liquid in …
Published in International Journal of Analytical and Applied Chemistry · Vol. 4, Issue 1, 2018 · pp. 1–7 Read article