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325 articles for “synthesis”
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SYNTHESIS AND IR-SPECTROSCOPIC STUDY OF MIXED LIGAND COMPLEX COMPOUNDS OF COPPER (II) FORMAT WITH SOME AMIDES
Abstract: Complex compounds of metals with amides, having biological activity are widely used in agriculture. Complex compounds of copper with organic ligands are physiologically active, participating in the vital processes of living organisms; the formiats have bactericidal and fungicidal properties. For the first time, mixed ligand complex compounds of copper (II) formate with formamide, thiocarbamide, acetamide and carbamide in an aqueous solution were synthesized. Using the methods of IR spectroscopy and …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 6, Issue 2, 2020 · pp. 31–38 Read article
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Experimental Study on Synthesis of Shear Thickening Fluid
Abstract: A novel class of nanosuspension material called shear thickening fluids (STFs) are created by dispersing micro- and nanoparticles in a dispersant. It is an intelligent material with excellent performance. When a modest shear rate is used, STFs are easily distorted. A material with noticeably improved characteristics is produced by this mixture (STF) of flowable and rigid components at a certain composition. Silica nanoparticles dispersed in a liquid polymer solution were …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 8, Issue 2, 2022 · pp. 1–6 Read article
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Synthesis of Low Cost Artificial Sand From Fly ash and its Application as a Filter Material
Abstract: The usage of natural river sand is increasing vastly. Geopolymers are materials with three-dimensional alumina silicate structures that have a high mechanical strength and can be used as an alternative to Portland cement. The probability of using Natural river sand can also be replaced with geopolymer synthetic sand. There are many properties which may lead the scarcity of natural riversand they are Because of landslides, tsunamis and erosion. The GPSS …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 8, Issue 2, 2022 · pp. 15–24 Read article
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Synthesis, Crystal growth and Characterization of Lead acetate zinc (II)Sulphate Material
Abstract: Leadacetatezinc (II) Sulphate Crystal is synthesized by the addition of Leadacetate to Zinc sulphate in equimolar concentration (1:1ratio) to produce larger sized crystal but during the crystallization process a bulk of colourless precipitate was obtained and after filtration the crystals are formed in the filtrate after slow evaporation solution growth technique. Thus formed crystals from the filtrate is kept away and the precipitate formed during the crystallization process is characterized …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 9, Issue 1, 2023 · pp. 22–29 Read article
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Thermodynamic Equilibrium Modeling of Sunflower Husk Gasifier to Produce Synthesis Gas
Abstract: Energy from biomass offers the great attraction in producing useful gaseous component resulting in low emissions and providing energy security. In the present study a gasifier model was developed using commercial Aspen Plus simulator. The model developed was based on the minimization of Gibb’s free energy and is validated with the experimental data of sunflower husk gasification using air as a gasifying agent. The results predicted are in good agreement …
Published in International Journal of Renewable Energy and its Commercialization · Vol. 2, Issue 2, 2016 · pp. 14–24 Read article
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Synthesis and Characterization of Mixed Ligand Complexes of Hydroxamic Acids with Metal (II) Phthalimide
Abstract: The mixed ligand complexes of Co (II) and Ni (II) with potassium salt of phthalimide (primary ligand) and hydroxamic acids (secondary ligand), where hoxm = L1=3,4,5-trimethoxy benzohydroxamic acids (TMBHA), L2=N-phenyl–3,4,5-trimethoxy benzohydroxamic acid (PTMBHA), L3=3,4-di methoxy benzohydroxamic acid (DMBHA) and L4=N-phenyl-3,4-di methoxy benzohydroxamic acid (PDMBHA) and phth=phthamlimide were synthesized and characterized by elemental analysis, melting points, I.R studies, UV–visible analysis, measurement of magnetic susceptibility, thin layer chromatography, etc. Elemental analysis depicts …
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 3, Issue 1, 2017 · pp. 1–6 Read article
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Green Synthesis of Silver Nanoparticles using Aqueous Leaf Extract of Artabotrys odoratissimus R.Br.
Abstract: In the present study silver nanoparticles were synthesized using the aqueous leaf extract of Artabotrys odoratissimus R.Br. as the reducing agent. The formation of silver nanoparticles was confirmed by colour change from light yellow to dark brownish red, UV-Visible Spectroscopy, FTIR, X-Ray Diffraction Method (XRD), Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray microanalysis spectroscopy (EDS). The nanoparticles showed an absorbance at 475.5nm on UV-Visible spectroscopy. Fourier Transform Infra-Red (FTIR) …
Published in International Journal of Applied Nanotechnology · Vol. 4, Issue 1, 2018 · pp. 5–11 Read article
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Synthesis and Characterization of CdS Nanoparticles for LED Application
Abstract: In the present work we have synthesized the size tuned CdS nanoparticles with chemical routes method. Size of the nanoparticle tuned with varying the addition of an appropriate quantity of capping agent. UV spectroscopy used to study the variation of optical properties with tuning the size of nanoparticle. EMA and TBM techniques are used to analyze size and band gap of the quantum dots.
Published in International Journal of Applied Nanotechnology · Vol. 4, Issue 1, 2018 · pp. 12–18 Read article
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Synthesis and Characterization of Fluorescent Core-Shell Ag@SiO2 and Ag@MoS2 Nanoparticle
Abstract: Among metals, silver (Ag) and gold (Au) NPs have attracted significant interest owing to their extraordinary optical properties related with the localized surface Plasmon resonance. However, the main drawbacks of colloidal nanoparticles, making them barely useable in the photovoltaic field, are their low colloidal stability. To overcome this problem we have developed a new class of fluorescent core-shell Ag@SiO2 nanoparticles, or simply called (MEF) nanoparticles. Different characterization techniques UV-Vis, PL …
Published in International Journal of Applied Nanotechnology · Vol. 5, Issue 2, 2019 · pp. 8–16 Read article
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Grafting of Starch: Synthesis and Thermal Properties
Abstract: Starch chloroacetate (St.ClAc) as a macro-initiator was pre-synthesized with reaction of primary OH groups on powder starch and characterized. In this study, the graft copolymer of St.ClAc with the previously synthesized 2-(4-methoxyphenylamino)-2-oxoethyl methacrylate (MPAEMA) and N-cyclohexylmethacrylamide (NCMA) monomer was made by atom transfer radical polymerization method (ATRP). St.ClAc and its graft copolymers (St.ClAc-g-MPAEMA and St.ClAc-g-NCMA) were characterized by FT-IR spectra and elemental analysis. In addition, thermal stability of these new …
Published in International Journal of Applied Nanotechnology · Vol. 6, Issue 1, 2020 · pp. 23–29 Read article
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Green Synthesis of Metallic Nanoparticles and Their Use as Nano Minerals in Poultry Nutrition
Abstract: Nanoparticles have become a part and parcel of our daily life in our food, refrigerators, cosmetics etc. However, in poultry production, the use of nanoparticles is still in their benign stage. Nano minerals have various implications in poultry production ranging from growth promotion, antioxidant activity, antimicrobial activity and reduced environmental pollution. The risks associated with nanoparticle handling, consumption and disposal are yet to be researched and a regulatory body is …
Published in International Journal of Applied Nanotechnology · Vol. 8, Issue 2, 2022 · pp. 32–36 Read article
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Synthesis and characterization of some organic semiconductor materials for optoelectronics
Abstract: Charge transfer complexes have high molar absorptivities and it’s an important phenomenon in the energy transfer process to increase the conductivity. Charge transfer complexes have been used in organic photovoltaic cells, organic semiconductors. Charge transfer complexes formed between electron donors and acceptors with strong interaction.In this paper, a Charge transfer complexes (CTC) of some organic semiconductor’s materials have been studied spectrophotometrically in chloroform, when the optical absorption of the CTC …
Published in International Journal of Energetic Materials · Vol. 6, Issue 1, 2020 · pp. 14–24 Read article
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A Brief Review of Simonkolleite Nanoparticles: Synthesis, Characterizations, and Their Transformative Impact Across Industries
Abstract: The rapid progress in nanotechnology has ignited a quest for innovative materials tailored to specific application needs or designed to enhance particular characteristics. Among these, simonkolleite, a zinc-based material, has emerged prominently in scientific discussions due to its promising properties with diverse medical, health, and environmental applications. This systematic review delves into the extensive literature on simonkolleite, unraveling its myriad applications across various fields. Often associated with ZnO-related research, Simonkolleite …
Published in International Journal of Energetic Materials · Vol. 9, Issue 1, 2023 · pp. 36–47 Read article
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Synthesis, Characterization and Biological Studies Using X-Beam Crystal Structures Which Utilizes (1) Cu Kα Data with Synchrotron Data
Abstract: The outcomes demonstrate that the complex responds as a bidentate ligand and is bound to the metal particle through the two oxygen iotas of the ligand (HL). The enactment energies, ΔE*, entropies ΔS*, enthalpies ΔH* and request of responses have been gotten from differential thermo-gravimetric (DTA) bends. In light of hindrance zone breadth estimations, the complex showed noteworthy antibacterial movement against both Staphylococcus aureus and Escherichia coli. It additionally displayed …
Published in International journal of Nanobiotechnology · Vol. 3, Issue 1, 2017 · pp. 1–5 Read article
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Green synthesis of Copper nanoparticles using Ctenolepis garcini (Burm.f.) C.B Clarke.
Abstract: Copper nanoparticles, due to the excellent physical and chemical properties and low cost of preparation, have been of great interest in wide applications as heat transfer systems, antimicrobial materials, super strong materials, sensors and catalysts. The present study is a novel biological approach for the formation of copper nanoparticles using Ctenolepis garcinii (Burm.f.) C.B Clarke. Copper nitrate was made to reduce with aqueous solution of plant extract. UV-Visible spectrum showed …
Published in International journal of Nanobiotechnology · Vol. 3, Issue 2, 2017 · pp. 1–6 Read article
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Synthesis of chitosan mediated nanoparticles and its antimicrobial activity
Abstract: In this study, chitosan nanoparticles were synthesized from chitosan polymer by ionic gelation method. The chitin was first extracted from crab shell and then deacetylated to chitosan. The presence and characterization of chitosan nanoparticles was investigated by UV-Visible Spectroscopy (UV) and scanning electron microscopy (SEM). The antimicrobial property of these chitosan nanoparticles were studied against E.coli, S.aureus, S.typhi, P.aureginosa, C.albicans and A.niger and compare with chitosan polymer. CSNPs showed higher …
Published in International journal of Nanobiotechnology · Vol. 3, Issue 2, 2017 · pp. 31–35 Read article
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Synthesis and characterization of Calcium Alginate Nanoparticle for Drug Delivery Application
Abstract: The polymeric nanoparticles (PNPs) are prepared from biocompatible and biodegradable polymers such as chitosan, gelatin, sodium alginate and albumin in size between 10-1000 nm where the drug is dissolved, entrapped, encapsulated or attached to a nanoparticle matrix. Their nanometer-size promotes effective permeation through cell membranes and stability in the blood stream. These smart PNPs are widely used as carriers in the pharmaceutical sector for controlled release in drug delivery. In …
Published in International journal of Nanobiotechnology · Vol. 4, Issue 2, 2018 · pp. 35–41 Read article
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Trichoderma Based Synthesis of Silver Oxide Nanoparticles, Their Characterization and Assessment of Antifungal Activity
Abstract: The fungal spore suspension of Trichoderma harzianum was used for the preparation of AgO nanoparticles. T. harzianum spore suspension acts as reducing and stabilizing agent for the fabrication of nanoparticles. The synthesized nanoparticles were characterized by X-ray diffractometry (XRD), scanning electron microscopy (SEM), energy dispersive X-analysis (EDAX) and transmission electron microscopy (TEM). The AgO nanoparticles were circular in shape with average diameter 10-20 nm. The AgO nanoparticles showed promising antifungal …
Published in International journal of Nanobiotechnology · Vol. 7, Issue 2, 2021 · pp. 19–25 Read article
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Chemical Vapor Deposition Synthesis of Nanostructures
Abstract: The present investigation reports some fascinating development of novel In2O3 nanostructures utilizing surrounding controlled substance vapor statement method within the sight of a firmly diminishing hydrazine encompassing. The examinations are methodicallly done by keeping both of the transporter gas stream rate or the source temperature steady, and differing the other. For each of the affidavits, the development is learned at three unique areas downstream. In this paper, we report the …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 3, Issue 1, 2017 · pp. 1–15 Read article
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Synthesis and Characterization of Cesium Intercalated Graphene Thin Film
Abstract: Graphene Oxide (GO) becomes promising two-Dimensional (2D) material in optoelectronics due to its sparkling properties. In preparation step we used Carboxylation of graphene and vacuum filtration to create the free standing thin film of cesium (Cs) intercalated GO. In this work we have synthesized cesium (Cs) intercalated GO thin films at different concentration (0.03, 0.05, 0.1 mol %) by using vacuum filtration method. The functional group present in synthesized thin …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 4, Issue 1, 2018 · pp. 8–16 Read article