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61 articles for “x-ray microscope”
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Structural, Optical, and Antibacterial Properties of NiCr₂O₄/NiO Nanocomposite Synthesized by a Facile Microplasma Electrochemical Process
Abstract: Nowadays increasing severity of environmental pollution and antibiotic resistance poses significant global challenges, particularly due to the accumulation of organic pollutants from industrialization and the proliferation of antibiotic-resistant bacteria, which jeopardize ecosystems and public health. To address these issues, the development of advanced nanocomposites with photocatalytic and antimicrobial properties is of paramount importance. This article reports the synthesis of NiCr₂O₄/NiO nanocomposite conducted in the current study via atmospheric pressure microplasma …
Published in International Journal of Composite and Constituent Materials · Vol. 10, Issue 2, 2024 · pp. 1–12 Read article
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Design and Optimization of Heterogeneous Catalysts for Green Chemistry Processes
Abstract: The design and optimization of heterogeneous catalysts are critical for advancing green chemistry processes, aiming to minimize environmental impact while maximizing efficiency. This study explores innovative strategies for the development of heterogeneous catalysts that facilitate environmentally benign reactions. By integrating principles of catalyst design, surface science, and reaction engineering, we aim to enhance catalytic performance, selectivity, and stability. Catalyst composition and structure, investigating novel materials, including metal-organic frameworks (MOFs), zeolites, …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 10, Issue 1, 2025 · pp. 42–48 Read article
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Effect of Ge and Pb Impurities on the Optical Properties of Amorphous (Sb2Se3)90Sn10 Thin Films
Abstract: The as prepared samples of [(Sb2Se3)90Sn10]95 M5 [M = Ge, Pb] chalcogenide system were amorphous as evidenced by X-ray diffraction studies. The optical band gap has been estimated with the help of Taucs relation for the as-deposited [(Sb2Se3)90Sn10]95M5 thin films. It is observed that the optical band gap increase with increase in the Ge and Pb content, which may be due to decrease in the density of defect states. This …
Published in International Journal of Metallurgy and Alloys · Vol. 6, Issue 1, 2020 · pp. 7–14 Read article
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Trichoderma Based Synthesis of Silver Oxide Nanoparticles, Their Characterization and Assessment of Antifungal Activity
Abstract: The fungal spore suspension of Trichoderma harzianum was used for the preparation of AgO nanoparticles. T. harzianum spore suspension acts as reducing and stabilizing agent for the fabrication of nanoparticles. The synthesized nanoparticles were characterized by X-ray diffractometry (XRD), scanning electron microscopy (SEM), energy dispersive X-analysis (EDAX) and transmission electron microscopy (TEM). The AgO nanoparticles were circular in shape with average diameter 10-20 nm. The AgO nanoparticles showed promising antifungal …
Published in International journal of Nanobiotechnology · Vol. 7, Issue 2, 2021 · pp. 19–25 Read article
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Synthesis & Characterization of Fe3O4 Nanoparticles for Thermal Sensing Application
Abstract: n this work, Synthesis and characterization of magnetite (Fe3O4) nanoparticles by the co-precipitation method has been done. These nanoparticles were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared (FTIR), UV-Visible spectroscopy (UV) and Thermogravimetry analysis (TGA/DSC). SEM image show morphology and porosity of material. The nanoparticles show quasi-spherical morphology with mean size around 37 nm. The XRD and FTIR confirmed the functionalization of the Fe3O4 nanoparticles. …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 3, Issue 2, 2017 · pp. 10–19 Read article
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Comparative Analysis of Characterization Techniques for Nanomaterial: Strengths and Limitation
Abstract: Nanomaterials have become extremely popular in numerous fields because of their exceptional properties and potential applications. However, characterizing these materials can be challenging due to their minute size and substantial surface area. Over the years, various characterization techniques have been developed to understand the physical, chemical, and structural properties of nanomaterials. In this review, we compare and analyze the strengths and limitations of commonly used characterization techniques for nanomaterials. Several …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 8, Issue 2, 2022 · pp. 34–41 Read article
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Thermal and structural properties of surface treated ragweed fiber reinforced biodegradable polylactic acid biocomposites
Abstract: Natural fiber-reinforced composites (NFRC) are becoming more popular as technological advance recognizes the need for eco-friendly materials. This work presents Giant ragweed (Ambrosia trifida) as a new composite reinforcement material into polylactic acid (PLA) matrix to form novel natural fiber-reinforced composites. Different types of retting techniques are utilized, and hydrogen peroxide retting is proven to provide the most optimized properties. The fibers are taken through subsequent extraction and grinding processes. …
Published in International Journal of Composite and Constituent Materials · Vol. 8, Issue 2, 2022 · pp. 13–31 Read article
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Effect of Coupling Agent on Organoclay Dispersion in Polyethylene/Organoclay Nanocomposites for Packaging Industry
Abstract: Low-density polyethylene (LDPE) is one of the most widely used polymers in various fields, but due to the hydrophobic nature of LDPE, it is hard to prepare an LDPE/clay nanocomposite. In this article, an LDPE/organoclay nanocomposite, which can be used in the packaging industry, was prepared by melt-blending organoclay with a polymer matrix (LDPE) and compatibilizer, low molecular weight oxidized polyethylene. The influences of organoclay, and compatibilizer during melt mixing …
Published in International Journal of Composite Materials and Matrices · Vol. 9, Issue 1, 2023 · pp. 1–11 Read article
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Bioethanol Production from Corncob Cellulosic Biomass: RSM and ANN based Optimization for Dilute Acid Pretreatment
Abstract: To increase the yield of fermentable sugars, the complexity of lignocellulosic biomass requires a pretreatment method. Dilute acid hydrolysis was used to efficiently pretreatment corn cobs. The aim of this study was to characterize corncob and investigate the effect of process parameters on total reducing sugar (TRS) yield during dilute acid hydrolysis pretreatment of corncob biomass. The morphology and microstructure of the samples were examined using an X-ray diffraction machine, …
Published in International Journal of Chemical Engineering and Processing · Vol. 9, Issue 2, 2023 · pp. 16–34 Read article
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Solution Combustion Synthesis of Yttrium molybdate (Y6MoO12) Nanoparticles by using Peroxomolybdic Acid, Characterization and Applications
Abstract: The main aim of our present research work is to synthesize the distinct yttrium molybdate (Y6MoO12) nanoparticles with excellent photocatalytic activity through ultra-rapid solution combustion route using peroxomolybdic acid as molybdenum source for the first time. The morphology of Y6MoO12 nanoparticles studied using scanning electron microscopy (SEM) exposes that the particles are exceedingly porous and agglomerated. From BET surface area measurement, it is examined that Y6MoO12 nanoparticles exhibit relatively large …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 7, Issue 1, 2021 · pp. 1–12 Read article
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Synthesis of Zero Valent Silver Nanoparticles by Chemical Reduction Method and its Application
Abstract: Chemical synthesis is one of the commonly used method for nanoparticles synthesis. Different chemicals acts as reducing agents which converts chemical precursor into its nano form. There are various chemical methods for the synthesis of zero valent silver nanoparticles. The silver nitrate is commonly used as precursor, sodium borohydride acts as reducing agent while sodium dodecyl sulphate stabilizes the formation of nanoparticles. The formation of silver nanoparticles was characterized by …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 7, Issue 2, 2021 · pp. 8–17 Read article
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Synthesis and Characterization of Polymer-Based Organic–Inorganic Hybrid Materials viaSol–Gel Processing: A Review of Gelatin–Silica, Gelatin–Silica–Titania and HPMA-Based Systems
Abstract: Organic–inorganic hybrid materials have emerged as a versatile class of advanced materials that integrate the flexibility and functionality of organic polymers with the thermal, mechanical, and chemical stability of inorganic networks. Among the available fabrication routes, the sol–gel process has gained considerable attention because of its simplicity, low processing temperature, compositional flexibility, and ability to tailor material properties at the molecular level. The present review discusses the synthesis and characterization …
Published in International Journal of Polymer Science and Engineering · Vol. 12, Issue 2, 2026 Read article
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UV-Spectroscopic Interaction Studies of Synthesized Graphene Oxide and Methyl Orange
Abstract: Graphene oxide (GO) has become a popular material due to its valuable properties and wide range of applications in various fields. GO was synthesized using a modified Hummers’ method and characterized through various techniques, including X-ray diffraction (XRD), and scanning electron microscopy (SEM), The effectiveness of GO in decolorizing methyl orange was assessed using UV-Vis spectrophotometry, with varying GO concentrations (0.05, 0.075, 0.1, 0.15) g and time (2–120 minutes) intervals. …
Published in International Journal of Environmental Chemistry · Vol. 10, Issue 2, 2024 · pp. 36–47 Read article
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Synthesis of Nano-ZnO by Chemical Method and its Characterization
Abstract: Nanocrystals of ZnO were prepared by chemical method using Zn (II) acetate and potassium hydroxide as the starting materials and methanol as solvent. The material was characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), electron diffraction analysis (EDS), UV-Visible spectroscopy, Dynamic light scatteringanalysis (DLS) and Fourier transform spectroscopy (FTIR) techniques. The results indicated that the obtained ZnO material was in nano-dimension and possessed pure …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 8, Issue 1, 2022 · pp. 13–18 Read article
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Synthesis, Crystal growth and Characterization of Lead acetate zinc (II)Sulphate Material
Abstract: Leadacetatezinc (II) Sulphate Crystal is synthesized by the addition of Leadacetate to Zinc sulphate in equimolar concentration (1:1ratio) to produce larger sized crystal but during the crystallization process a bulk of colourless precipitate was obtained and after filtration the crystals are formed in the filtrate after slow evaporation solution growth technique. Thus formed crystals from the filtrate is kept away and the precipitate formed during the crystallization process is characterized …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 9, Issue 1, 2023 · pp. 22–29 Read article
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Green synthesis of Copper nanoparticles using Ctenolepis garcini (Burm.f.) C.B Clarke.
Abstract: Copper nanoparticles, due to the excellent physical and chemical properties and low cost of preparation, have been of great interest in wide applications as heat transfer systems, antimicrobial materials, super strong materials, sensors and catalysts. The present study is a novel biological approach for the formation of copper nanoparticles using Ctenolepis garcinii (Burm.f.) C.B Clarke. Copper nitrate was made to reduce with aqueous solution of plant extract. UV-Visible spectrum showed …
Published in International journal of Nanobiotechnology · Vol. 3, Issue 2, 2017 · pp. 1–6 Read article
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Mechanical and Microstructure Properties of Al and SiC Reinforced Aluminum-Based Metal Matrix Composite
Abstract: It is becoming increasingly difficult to design new technical materials that are resistant to wear damage and corrosion degradation in severe service circumstances. Unfortunately, even with crucial passive metals, like Al alloys, there is often a compromise between wear and corrosion resistance. Because of the unfavorable galvanic connection between the precipitates and the matrix, precipitates not only harden the material but also accelerate corrosion. This research established that a supersaturated …
Published in International Journal of Metallurgy and Alloys · Vol. 11, Issue 1, 2025 · pp. 26–43 Read article
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Low temperature plasma treatment of polymeric membranes: a comparative review
Abstract: This paper presents a comparative study of plasma surface modification of various polymeric membranes. Low temperature plasma treatment using pulsed direct current discharge of different gases was employed to enhance hydrophilicity of membranes. Radio frequency discharge of various gases was used to improve surface properties of different polymeric membranes. The enhancement of hydrophilicity of the plasma modified membrane surface was evaluated by measuring the contact angle. The membranes were characterized …
Published in International Journal of Polymer Science and Engineering · Vol. 6, Issue 1, 2020 · pp. 1–19 Read article
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Chemical Synthesis and Characterization of Polyaniline for Supercapacitors Application
Abstract: Various polyaniline (PANI) synthesis methods are reported in the literature, depending on the experimental parameters involved (T, t, doping, and mixing procedure). Herein, three chemical polymerization methods were used to synthesis PANI from aniline monomer: rapid oxidation (OR), controlled oxidation (CO), and interfacial oxidation (OI). The PANI was therefore deposited next by drop casting on a silicon (Si) substrate. X-ray diffraction, Raman spectroscopy, and scanning electron microscopy were used to …
Published in International Journal of Chemical Engineering and Processing · Vol. 8, Issue 2, 2022 · pp. 9–16 Read article
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A Comprehensive Characterization of Zinc Chloride: Unveiling its Role as a Hygroscopic Preservative and Drying Agent through Elemental, Structural, and Morphological Analysis
Abstract: This study presents a detailed investigation of Zinc Chloride( )) utilizing the following different analytical techniques, X-ray diffraction(XRD), Electron Dispersive Spectroscope (EDS), Transmission Electron Microscope (TEM), Scanning Electron Microscope (SEM). Zinc Chloride was synthesized using the hydrothermal method. The elemental, structural, morphological, and optical properties of Zinc Chloride ( )) were thoroughly analyzed. The hygroscopic nature and properties of Zinc Chloride upon exposition to air was revealed and its weight/mass …
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 9, Issue 2, 2023 · pp. 13–19 Read article