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78 articles for “Ethanol.”
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Hydrogenation of dimethyl-nitrobenzene to dimethyl-aniline in a three-phase Reactor
Abstract: The liquid-phase catalytic hydrogenation of dimethyl-nitrobenzene (DN) to Dimethyl-aniline (DA) was carried out in ethanol using 5% Pd/C as a catalyst. The effects of hydrogen partial pressure (400–1000 kPa), reaction temperature (343–403 ), catalyst loading (5–15 g/lit), speed of stirring range (200-800 rpm) and dimethyl-nitrobenzene concentration (0.12–0.75 mol/lit) on the hydrogenation of dimethyl-nitrobenzene and the yield of Dimethyl-aniline have been studied. Dimethyl-aniline was the only reaction product, generated through the …
Published in International Journal of Chemical Separation Technology · Vol. 3, Issue 2, 2017 · pp. 1–13 Read article
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Synthesis, Characterization and Optimization of Essential Oil from Pumpkin Seed
Abstract: The main aim of this research work was extraction, characterization and optimization of essential oil from pumpkin seed, cucurbita pepo variety using ethanol as a solvent. The extraction was carried out by using a Soxhlet, leaching method and oil was separated from solvents by using rotary evaporator. Pumpkin seed was analyzed for proximate analysis and found that moisture content of 5.21 , crude proteins content of 22.50.31%, crude fat content …
Published in International Journal of Chemical Separation Technology · Vol. 7, Issue 1, 2021 · pp. 6–27 Read article
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Studies on Phytochemical analysis of Areca Palm Leaves
Abstract: Areca palm plant is commonly known as Palm trees and belongs to the family Arecaceae. Probablyone of the best and frequently grown plant families is the palm family. Palm trees are cultivating in South America, South Pacific area, Southern Asia, and Arabic countries etc. The greatest number of palm species may exist in Colombia. Palms are used to make a wide variety of everyday goods and cuisines. This palm plant …
Published in International Journal of Chemical Separation Technology · Vol. 8, Issue 1, 2022 · pp. 1–11 Read article
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Catalytic hydrogenation of dimethyl-nitrobenzene to dimethyl-aniline over Ni catalysts
Abstract: The catalytic transfer hydrogenation of dimethyl-nitrobenzene (DN) to Dimethyl-aniline (DA) was studied in the temperature range 343–403 , pressure range of 4–10 bar H2 and ethanol as solvent using Ni on alumina-silicate as catalyst above agitation speed 800 rpm. The substrate feed concentration was varied in the range from 0.124 to 0.745 kmol/m3 while catalyst loading was in the range 4–12% (w/w) of dimethyl-nitrobenzene. Dimethyl-aniline was the only reaction product, …
Published in International Journal of Chemical Engineering and Processing · Vol. 3, Issue 2, 2017 · pp. 19–29 Read article
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Cassia Fistula Leaf and Flower Extract and their Antibacterial Activity: A Comparative Study
Abstract: Overwhelming side effects of synthetic drugs has attracted researchers for the search and use of herbal drugs. Neem and Curcumin are very widely studied and research is still going on these species. However, Cassia Fistula, is one such plant which has various medicinal values and is less studied. Thus, the present investigation studies the extraction of leaf and flower constituents and the extract has been characterized by FTIR and NMR …
Published in International Journal of Chemical Engineering and Processing · Vol. 5, Issue 1, 2019 · pp. 1–10 Read article
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A New Multidentate Fluorescent Chemosensor for metal ions: Synthesis and Fluorescence Response
Abstract: We report the synthesis and the fluorescence response to metal ions of a multidentate pyridyl-based ligand in MeCN/H2O (3/7) solution. The ligand was synthesided via overnight refluxing of a ethanolic mixture of 2,6-diamino pyridine and di(pyridine-2-yl)methanone. studies reveal the ligand display sensing response ability in the presence of certain metal ions. It display significant fluorescent quenching in the presence of Ni2+, Co2+, Zn2+ and Cd2+, with remarkable fluorescence “turn-off” response …
Published in International Journal of Environmental Chemistry · Vol. 5, Issue 1, 2019 · pp. 10–17 Read article
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Preparation and Characterisation of the Schiff’s Base Complex [Pt(dpq)Cl2]
Abstract: Preparation of platinum complex [Pt(dpq)Cl2] and characterization of the complex by IR, UV, CHN and NMR techniques. DPQ ligand is obtained by 1,10 phenanthroline made react with NaBr, nitrating mixture followed by ethylenediamine in ethanol. Keywords: DPQ, intercalator, platinum complex, Schiff’s base
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 1, Issue 2, 2015 Read article
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Synthesis, characterization of Schiff base and its pH metrically studies of transition metal complexes of N'-(3, 4-dihydroxybenzylidene) isonicotinohydrazide.
Abstract: Schiff reaction is one of the versatile reaction widely used in organic synthesis focused on the discovery & development of isoniazide Schiff base derivative N’(3,4-Dihydroxy benzylidene isonicotinohydrazide) have been reported in presence of 0.01g molecular iodine catalyst stirring give fast product & good yield. The synthesized compound is characterized by FTIR & H-NMR analysis. For the development of coordination chemistry Schiff base & metal ion having played most important role, …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 6, Issue 2, 2020 · pp. 39–47 Read article
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Synthesis of Various Products from Different Feed Stocks–an Insight Into Application of Biotechnology
Abstract: Synthesis of various products in energy efficient manner with minimum environmental foot print is important area of research in chemical engineering. Chemical pathways are energy intensive and many of the reactions are high temperature reactions. Many compounds like ethanol, amino acids, and acetic acids can be synthesized by biological methods. Biochemical reactions are low temperature reactions under mild conditions. Use of waste material as feedstock for production of useful compounds …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 7, Issue 2, 2021 · pp. 18–21 Read article
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Studies on Fuel potential of different generation biofuels
Abstract: Ever-increasing pressing issue has been to generate biofuel energy for transportation, food security etc. Our nation has been continuously laying efforts in this field to develop methods that can provide sustainable energy source that can fulfill the growing needs. Fossil fuels which were earlier the only source of energy production is now been replaced by various other sources including algal strains. The latter has come forward as an alternate to …
Published in International Journal of Renewable Energy and its Commercialization · Vol. 3, Issue 1, 2017 · pp. 26–29 Read article
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Catalytic Steam recycle of Bio-Oil Produces Hydrogen
Abstract: The "water-gas shift reaction" is a process that combines the vapour and carbon monoxide to produce carbon dioxide and more hydrogen.Steam reforming of actual bio-oil is a more realisticmethod for producing H2 despite substantial research on the heat reform of model compounds (such as ethanol). With a focus on the creation of catalysts for the procedure, this paper covers current developments in the steam reforming of actual bio-oil. Given its …
Published in International Journal of Renewable Energy and its Commercialization · Vol. 8, Issue 1, 2022 · pp. 25–29 Read article
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Preparation of Beta Lactam Compounds and Study of Thermodynamically Behavior
Abstract: Several Lactam derivatives have been prepared by condensation reaction of folic acid with (4-chloroacetophenone and 4-hydroxyacetophenone) in ethanol. Then the resultant compounds (1,2) react with another Schiff bases by reacting of 4- bromobenzaldehyde with an amino acid (Phenylalanine, Tryptophan, Tyrosine and Histidine) to give bis-β-lactam rings. The structures of target compounds were characterized by many spectroscopic methods including NMR, FTIR technique and their melting points. The β- lactam derivatives were …
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 5, Issue 2, 2019 · pp. 9–15 Read article
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Thermodynamic and Kinetic Characterization of Aluminum Corrosion and Inhibition Adsorption of Vernonia Amygdalina Fruit Extract IN 0.5N H2SO4
Abstract: Anti-corrosive efficacy of ethanolic extract of Vernonia amygdalina fruit extract on corrosion of aluminum in 0.5N H2SO4 acidic solution was explored by mass loss measurement at rise in temperature between 303-343 K for 24 hours immersion period. The I.E. (η%) has been noticed prominently high (62.92%) at concentration 0.45% at 303 K. An inhibitor adsorption on the surface aluminum have been found to be best fitted Langmuir adsorption isotherm. It …
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 9, Issue 1, 2023 · pp. 20–27 Read article
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Modern Ceramic Compose to Pervade Electronics
Abstract: This article composed from articles where ceramics, photonics, and allied fame schemed. Scheme of materials is studied to transduce optical, electrical, mechanical, and magnetic phenomenon. Evolution of description at nanometer level of distributing from non-degenerating phases schemed ferrite in the ferroelectric matter to subject magnetic memory contravened from/by electrostatic to electrical current preserved memory acts. Suggestive selective scriptive as from magneto-electric effect induced dielectric polarization of material under effects of …
Published in International Journal of Metallurgy and Alloys · Vol. 7, Issue 2, 2021 · pp. 11–16 Read article
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Studies of Technical Grades from Rice Husks
Abstract: Rice husks studied in this review to subject different accessible performance in lieu of abated the dispose with no pollution. Rice husk ash in mesoporous form added in soap during preparation. Other formations appeared to process for ceramics, catalysts, adsorbing material, nano-mater and carbon added cementation products. Rice husk is by-product from rice mill subjectively reused to access another staged mission to form by-products. Firing of rice husk studied other …
Published in International journal of Nanobiotechnology · Vol. 6, Issue 2, 2020 · pp. 25–30 Read article
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Study of Dynamic Mechanical and Thermal Properties of Poly(Ether Ether Ketone) Carbon Nanotubes
Abstract: The effect of polyetherimide (PEI) as a compatibilizing agent on the morphology, thermal, electrical and dynamic-mechanical properties of poly(ether ether ketone) (PEEK)/single-walled carbon nanotube (SWCNT) nanocomposites, has been investigated for different CNT loadings. After a pre-processing step based on ball milling and premixing under mechanical treatments in ethanol, the samples were prepared by melt extrusion. A more homogeneous distribution of the CNTs throughout the matrix is found for composites containing …
Published in International Journal of Polymer Science and Engineering · Vol. 3, Issue 1, 2017 · pp. 1–21 Read article
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Experimental Demonstration on the Recording of Capillary-Filled Microfluidic Devices Fabricated by Polymeric Material
Abstract: In this present experimental work, total 52 individual PMMA microfluidic devices are fabricated by maskless lithography, hot embossing lithography and direct bonding technique in a cleanroom laboratory. The selected working liquids are dyed water, dyed aqueous ethanol and dyed aqueous isopropyl alcohol and are prepared in a materials-science laboratory. Fabricated microfluidic devices are tested by the prepared aqueous working liquids, and each capillary-filled device after the surface-driven microfluidic flow is …
Published in International Journal of Polymer Science and Engineering · Vol. 5, Issue 2, 2019 · pp. 31–41 Read article
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Experimental Studies on the Surface-Driven Microfluidic Flow of Dyed Working Liquids in Sudden Expansion Microchannels Fabricated by Polymer
Abstract: In this experimental work, the sudden expansion microchannels are fabricated by maskless lithography, hot embossing lithography, drilling, direct bonding technique and chip separation technique using own hands-on of author completely. Total 15 individual sudden expansion microchannels are fabricated in this work using polymethylmethacrylate (PMMA) as optically transparent polymer. Effects of channel aspect ratio, surface wettability and liquid viscosity on surface-driven microfluidic flow are experimentally studied in the fabricated sudden expansion …
Published in International Journal of Polymer Science and Engineering · Vol. 6, Issue 1, 2020 · pp. 44–59 Read article