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136 articles for “Crystal”
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Synthesis, Crystal Growth and Characterization of Bismuth Doped Potassium Hydrogen Phthalate Crystal (Khp): A Nlo Material
Abstract: To create single crystals using the Slow Evaporation Solution Growth Technique (SEST), equimolar composition of the transition metal (Bi) as Bismuth nitrate is added to Potassium Hydrogen Phthalate (KHP) (1:1) at ambient temperature. The following analysis is then performed on the single crystals that have formed. Equimolar doping-induced structural distortion in the crystals is confirmed by the FT-IR Spectra. The TGDTA study reveals the purity of the material and no …
Published in International Journal of Composite Materials and Matrices · Vol. 10, Issue 1, 2024 · pp. 19–27 Read article
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Crystal Growth, Synthesis and Characteristic Studies of Bismuth Doped Tristhioureazinc (II) Sulpate (ZTS) Crystal
Abstract: Potential semi organic tristhioureazinc(II) sulphate (ZTS), One of the best room temperature growth techniques for nonlinear optical materials with high SHG efficiency is slow evaporation solution growth, which produces pure and single crystals for use in laser technology and photonic applications. Single crystals Doping of Bismuth fluoride (equimolar) to ZTS is done during the crystallization process is further analysed by single crystal XRD which infers that the Bismuth doped ZTS …
Published in International Journal of Chemical Separation Technology · Vol. 9, Issue 2, 2023 · pp. 45–52 Read article
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Advances in the Synthesis and Functional Applications of Crystalline Materials
Abstract: Crystalline materials represent one of the most important classes of advanced materials in modern science and engineering due to their highly ordered atomic arrangements and outstanding physical, chemical, electrical, optical, thermal, and mechanical properties. The periodic organization of atoms within crystal lattices provides exceptional opportunities for controlling and optimizing material performance through advanced synthesis strategies, crystal growth techniques, compositional modification, and defect engineering. Recent progress in materials science has enabled …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 12, Issue 2, 2026 Read article
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Separation of p-xylene from xylene isomer mixtures within a single stage porous batch cooling crystallizer
Abstract: Crystallization based separation of p-xylene from its isomer mixtures were mostly accomplished in stirring crystallizers, suspension crystallizer and scrapping crystallizer followed by centrifugation. In this work, separation process for p-xylene, where both crystallization and separation of p-xylene in a single batch crystallizer, was performed. Upon cooling, p-xylene, which has the higher melting point than other xylene isomers (o-xylene and m-xylene), crystallizes first. Xylene mixture samples were crystallized at a lower …
Published in International Journal of Chemical Engineering and Processing · Vol. 6, Issue 1, 2020 · pp. 62–78 Read article
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Photonic Crystals – A Review
Abstract: Photonic crystals are periodically arrayed electromagnetic media, commonly having possessing photonic band gaps: ranges of frequency in which light cannot propagate through the structure. This periodicity, where the length scale is proportional to the wavelength of light in the band gap, is the electromagnetic analogue of a crystalline atomic lattice, where the latter acts on the electron wave function to make the familiar band gaps, semiconductors, and so on, of …
Published in International Journal of Plant Biotechnology · Vol. 4, Issue 1, 2018 · pp. 12–15 Read article
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Revolutionizing Glass Science: Analyzing the Crystallization Dynamics of Economical Glass-Ceramic Compositions
Abstract: The development of glass-ceramics presents an innovative approach to material science, leveraging the unique properties of non-crystalline glass combined with controlled crystallization. This study investigates the crystallization dynamics of economical glass-ceramic compositions derived from raw materials, such as blast furnace slag and granite rock. We explore the fabrication processes, examining the influence of these raw materials on microstructural interlocking and phase composition. Our findings reveal that specific ratios of slag …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 10, Issue 2, 2025 · pp. 9–15 Read article
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Effect of Sulphamic acid on the growth of Glycine single crystals
Abstract: Sulphamic acid added glycine single crystals were grown successfully by slow-evaporation technique.A single crystal with well defined crystal was obtained. The lattice parameters and crystal system of the grown crystals were confirmed by single crystal and powder x-ray diffraction analysis.The functional groups present in the sample were identified by FTIR spectral analysis.The lower cut off wavelength and bandgap energy of the grown crystal was analysed from uv-vis spectral analysis. Keywords: …
Published in International Journal of Energetic Materials · Vol. 5, Issue 1, 2019 · pp. 9–13 Read article
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Crystals (Thermotropic phases and Lyotropic phases) in Physical Properties
Abstract: In the current years there has been a cumulative growth to add the numerous nanomaterials to liquid crystals which is encouraged via frequent elements of resources advance. (i) accumulation of nanomaterials can conversion and thus melody the belongings of the liquid crystal (ii) inventive functionalities can be added to the liquid crystal (iii) the self-organization of the liquid crystalline formal can be abused to pattern systematic structures or to assignment …
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 5, Issue 2, 2019 · pp. 16–22 Read article
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Numerical Analysis of Flow Characterization in a Continuous Crystallizer
Abstract: In this work, hydrodynamics in a draft tube continuous crystallizer is analyzed computationally through Ansys CFD to crystallization phenomena. Hindrance to fluid mixing and particle suspension due to vortexing can be overcome by providing baffles. A draft tube ensures that it directs the flow in vertical direction ensuring good axial blending. Here CFD simulations are performed using multiple reference frame (MRF) with sliding mesh approach in transient condition for flow …
Published in International Journal of Chemical Separation Technology · Vol. 2, Issue 2, 2016 · pp. 33–43 Read article
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Synthesis, Crystal growth and Characterization of Lead acetate zinc (II)Sulphate Material
Abstract: Leadacetatezinc (II) Sulphate Crystal is synthesized by the addition of Leadacetate to Zinc sulphate in equimolar concentration (1:1ratio) to produce larger sized crystal but during the crystallization process a bulk of colourless precipitate was obtained and after filtration the crystals are formed in the filtrate after slow evaporation solution growth technique. Thus formed crystals from the filtrate is kept away and the precipitate formed during the crystallization process is characterized …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 9, Issue 1, 2023 · pp. 22–29 Read article
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Solid state Acid–Base Reactions of Arylamino Nicotinic Acids: X-ray Crystal Structures of Salts
Abstract: 2-(Phenylamino)nicotinic acid (PNA), 2-(methyl(phenyl)amino)nicotinic acid (MPNA), 2-(p-tolylamino)nicotinic acid (TNA) and 2-(methyl(p-tolyl)amino)nicotinic acid (MTNA) are the ampholites which were synthesized by the coupling of respective aryl amines and 2-chloronicotinic acid in the presence of p-tolylsulfonic acid and pyridine. All these molecules were crystallized in different solvents to obtain intra and intermolecular proton transferred adducts in the solid state. TNA is an only compound which has under gone intra (zwitterion) and intermolecular …
Published in International Journal of Analytical and Applied Chemistry · Vol. 1, Issue 2, 2015 · pp. 1–11 Read article
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RECENT DEVELOPMENTS ON VOLATILE DEEP EUTECTIC SOLVENTS FOR APPLICATION IN CRYSTALLIZATION OF PHARMACEUTICAL COMPOUNDS.
Abstract: Crystallization is one of the most effective separations and purification methods used in the pharmaceutical and fine chemical industries. Volatile organic solvents are widely used in the crystallization of pharmaceutical compounds. Some properties of these solvents such as volatility, instability, combustibility,unpredictable nature, and toxicity are undesirable. In therecent years solvents known as ionic liquids and deepeutectic solvents (DES) derived from ionic liquidsgain importance due to the interesting properties as solvents. …
Published in International Journal of Chemical Separation Technology · Vol. 8, Issue 1, 2022 · pp. 20–26 Read article
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Numerical investigation of hydrodynamics of batch crystallizer
Abstract: In this work, hydrodynamics in a draft tubebatch crystallizer is analysed computationally using Computational fluid dynamics (CFD). The CFD simulations are performed using multiple reference frame (MRF) with sliding mesh approach in transient condition for flow time of 5s using the standard k-ε turbulence model. The flow-field in batch crystallizer is quantified by calculating time averaged velocity profiles along the horizontal line and by analysing the temporal variation of liquid …
Published in International Journal of Chemical Engineering and Processing · Vol. 3, Issue 1, 2017 · pp. 24–35 Read article
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Mechanical Studies and Thermal Kinetics of Isoniazid Crystals
Abstract: Single crystals of isoniazid were crystallized by slow solvent evaporation method. The crystal structure was confirmed using single crystal X-ray diffraction analysis. Micro hardness was estimated and work hardening coefficient and Newtonian resistance pressure of the crystal were determined. Kinetic analysis of the thermogravimetric data was carried out by using Coats-Redfern relation. Activation energy, frequency factor and order of reaction were also calculated. Arrhenius equation for isoniazid is k=0.43×105e–79103/RT mol–1s–1. …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 1, Issue 1, 2015 Read article
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Study of optical properties for five ring hexagonal photonic crystal fiber
Abstract: In this paper, basically, we have investigated about different optical properties for five-ring hexagonal photonic crystal fiber. Silica glass as material for PCF is taken and different parameters analyzed like, Effective refractive index, confinement loss and Waveguide dispersion. Properties are analyzed by varying the key design parameters like air hole diameter and lattice pitch. The comparative study of the results for different design parameters is analyzed. It has been observed …
Published in International Journal of Composite and Constituent Materials · Vol. 5, Issue 1, 2019 · pp. 28–33 Read article
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Reactor-Made Polypropylene for 3D Printing: A Low-Crystallinity Approach
Abstract: 3D printing is technology that enables the complex structure, which is difficult in conventional technique. However, relatively slow manufacturing process and using of limited polymeric material leads to attention of scientist towards newer cost-effective material and technology. In this study, we overcome this issue by synthesizing reactor-made polypropylene (mPP) using Dimethylsilylene-(cyclopentadienyl) (fluorenyl)-zirconium-dichloride metallocene catalyst. The polymerization process was systematically optimized by varying Al/Zr molar ratios, catalyst concentrations, and temperatures to …
Published in International Journal of Polymer Science and Engineering · Vol. 11, Issue 2, 2025 · pp. 1–17 Read article
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Thermal Decomposition Kinetics of Mefenamic Acid Crystals
Abstract: Single crystals of mefenamic acid were crystallized by gel growth method for the first time in literature. Crystal structure was confirmed using single crystal X-ray diffraction analysis. Kinetic analysis was made from the isothermal thermogravimetric analysis/differential thermal analysis (TGA/DTA) data using Coats–Redfern (CR) relation. Thermodynamic parameters were also determined. Arrhenius equation for mefenamic acid is k = 0.28 × 109 e–116551/RT mol–1s–1. Keywords: kinetic analysis, mefenamic acid, thermal analysis
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 2, Issue 1, 2016 · pp. 21–24 Read article
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Effect of Benzyl Triphenyl Phosphonium Chloride on Crystallization, Rheological Behaviour and Electrical Properties of Polypropylene and Polypropylene Grafted Maleic Anhydride
Abstract: The effect of benzyl triphenyl phosphonium chloride (BTPC) on polypropylene (PP) and polypropylene grafted maleic anhydride (PP-g-MA) in the proportions of 0-5% by weight studied in detail. PP/BTPC and PP/PP-g-MA/BTPC composites were produced by melt processing technique using twin screw microcompounder. Change in the force inside screw barrel during melt mixing of PP based composites were recorded. The prepared composites were analysed using rheometer, differential scanning calorimetry and hot stage …
Published in International Journal of Composite Materials and Matrices · Vol. 7, Issue 1, 2021 · pp. 45–52 Read article
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Synthesis, Characterization and Biological Studies Using X-Beam Crystal Structures Which Utilizes (1) Cu Kα Data with Synchrotron Data
Abstract: The outcomes demonstrate that the complex responds as a bidentate ligand and is bound to the metal particle through the two oxygen iotas of the ligand (HL). The enactment energies, ΔE*, entropies ΔS*, enthalpies ΔH* and request of responses have been gotten from differential thermo-gravimetric (DTA) bends. In light of hindrance zone breadth estimations, the complex showed noteworthy antibacterial movement against both Staphylococcus aureus and Escherichia coli. It additionally displayed …
Published in International journal of Nanobiotechnology · Vol. 3, Issue 1, 2017 · pp. 1–5 Read article
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Highly Birefringence and Flattened Dispersion Photonic Crystal Fiber for Polarization Maintaining
Abstract: In this paper we present flattened dispersion and highly birefringence photonic crystal fiber. Higher Birefringence is required in sensing to maintain the linear polarization by reducing polarization coupling. The Flattened dispersion is used broadband and telecommunication application. This paper structure is hexagonal pcf with circular air-holes and we calculate the pcf property like effective index, dispersion, birefringence, confinement loss. This PCF is designed by COMSOL Multiphysics Software.
Published in International Journal of Composite and Constituent Materials · Vol. 5, Issue 1, 2019 · pp. 22–27 Read article