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85 articles for “XRD”
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Correlation between full width at half maximum (FWHM) of XRD peak with mechanical properties
Abstract: Full width at half maximum (FWHM) of XRD profiles characterizes different mechanical properties. However, there is no literature available that discusses about the correlation between the FWHM of XRD peaks with mechanical properties (ultimate tensile strength, yield strength, strain hardening coefficient and micro-hardness) upon plastic deformation. Martensitic stainless steel (type 410) and Ferritic stainless steel (type 430) samples were plastically deformed under different strain rate using tensile testing machine. Variation …
Published in International Journal of Metallurgy and Alloys · Vol. 1, Issue 1, 2015 · pp. 15–23 Read article
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Green Synthesis of Silver Nanoparticles from Trapa bispinosa Fruit Extract: Characterization and Promising Antimicrobial Activity Against Multidrug-Resistant Pathogens
Abstract: Silver nanoparticles (Ag NPs) are widely recognized for their applications in medicine, electronics, and environmental remediation. This study presents a new green synthesis method for Ag NPs using Trapa bispinosa fruit extract as a natural reducing agent and stabilizing agent. Characterization of the synthesized Ag NPs through X-ray diffraction (XRD) confirmed a crystalline structure consistent with the face-centered cubic (fcc) arrangement, with peaks at (111), (200), (220), (311), and (222), …
Published in International Journal of Applied Nanotechnology · Vol. 11, Issue 1, 2025 · pp. 38–46 Read article
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Green Synthesis of Silver Nanoparticles using Aqueous Leaf Extract of Artabotrys odoratissimus R.Br.
Abstract: In the present study silver nanoparticles were synthesized using the aqueous leaf extract of Artabotrys odoratissimus R.Br. as the reducing agent. The formation of silver nanoparticles was confirmed by colour change from light yellow to dark brownish red, UV-Visible Spectroscopy, FTIR, X-Ray Diffraction Method (XRD), Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray microanalysis spectroscopy (EDS). The nanoparticles showed an absorbance at 475.5nm on UV-Visible spectroscopy. Fourier Transform Infra-Red (FTIR) …
Published in International Journal of Applied Nanotechnology · Vol. 4, Issue 1, 2018 · pp. 5–11 Read article
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Structural and Optical Study of CdSe Q-dots
Abstract: In this paper we have report the properties of CdSe Q-dots. Calculations of different parameters for different sizes of CdSe Q-dots are presented. The XRD analysis used to find the composition, crystal structure and crystallite size. Scherrer equation is used to calculate the Nano crystallite size. XRD analysis reveals that the CdSe QD crystallite sizes in the sample are 3.26 nm, 3.72 nm, and 3.20 nm by applying the appropriate …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 8, Issue 1, 2022 · pp. 25–30 Read article
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Biosynthesis of Silver Nanoparticles using Aqueous Extract of Chaetomorpha media (C.Ag.) Kuetzing
Abstract: Chaetomorpha media (C.Ag.) Kuetzing is common green seaweed belongs to the family Chlorophyceae. The aqueous extract of Chaetomorpha media was used for the biosynthesis of Silver Nanoparticles. The Silver Nanoparticles were formed due to the reduction of silver nitrate to aqueous silver ions in the presence of seaweed extract. Silver nanoparticles exhibited dark brown colour in aqueous solution. The synthesized silver Nanoparticles were characterized by UV-Visible Spectrophotometer, Fourier Transform Infrared …
Published in International journal of Nanobiotechnology · Vol. 6, Issue 2, 2020 · pp. 12–18 Read article
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Effect of Calcium doping on Structural and Morphological properties of YBCO Superconductor
Abstract: In this paper, we have reported the effect of Ca doping in YBCO superconductors with an aim of understanding the effect of novel local nano distortions on the superconducting properties of YBCO. Solid state reaction method is used to prepare the samples. X-Ray diffraction pattern shows that the samples are polycrystalline and having orthorhombic structure while Resistivity measurement shows that Tc decreases with increase in Ca-doping.Morphological studies reveals clear evolution …
Published in International Journal of Applied Nanotechnology · Vol. 6, Issue 1, 2020 · pp. 6–10 Read article
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Value Addition of Quartz Gemstones through Gamma Irradiation
Abstract: Color enhancement of gemstones through gamma irradiation is an established technology throughout the world. By value addition, the traders earned manifold prices to these colorless stones as compared to the fresh ones. For the color enhancement of these semi-precious stones, optimized doses of irradiations are required. To get the optical properties of the stones and to investigate the crystal lattice and chemical composition, X-Ray diffraction (XRD) and energy dispersive X-ray …
Published in International Journal of Energetic Materials · Vol. 5, Issue 2, 2019 · pp. 61–67 Read article
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Auxiliary Characterization of (Co, Mn) Co-doped Zinc Oxide Thin Films
Abstract: Cobalt and manganese are both co-doped with zinc oxide films were set up by sol-gel turn covering strategy on quartz substrate by shifting the dopants focus. The result of dopants focus was researched by x-beam diffraction (XRD). The XRD design demonstrates that the kept movies have polycrystalline hexagonal wurtzite structure. SEM micrograph demonstrates the adjustments in morphology of very thin film as dopants fixation are fluctuating. The compositional examination did …
Published in International Journal of Metallurgy and Alloys · Vol. 2, Issue 1, 2016 · pp. 31–35 Read article
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An Analytical Study of Structural Optical Properties of CaAl2O4 Phosphors by Sol–Gel Method
Abstract: A comparative study of structure, morphology and optical properties of CaAl2O4 Phosphors by In this paper, monoclinic CaAl2O4 phosphor with various weight rate of aluminum was blended by low temperature sol–gel technique. The readied tests were described by X-beam diffraction (XRD) examination, Fourier change infrared (FTIR), checking electron microscopy (SEM), vitality dispersive spectroscopy (EDS) and photoluminescence discharge spectra (PL). The XRD examination demonstrated that CaAl2O4 have monoclinic structure. The normal …
Published in International journal of Nanobiotechnology · Vol. 2, Issue 1, 2016 · pp. 1–4 Read article
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Synthesis & Characterization of Fe3O4 Nanoparticles for Thermal Sensing Application
Abstract: n this work, Synthesis and characterization of magnetite (Fe3O4) nanoparticles by the co-precipitation method has been done. These nanoparticles were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared (FTIR), UV-Visible spectroscopy (UV) and Thermogravimetry analysis (TGA/DSC). SEM image show morphology and porosity of material. The nanoparticles show quasi-spherical morphology with mean size around 37 nm. The XRD and FTIR confirmed the functionalization of the Fe3O4 nanoparticles. …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 3, Issue 2, 2017 · pp. 10–19 Read article
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SYNTHESIS, CHARACTERIZATION AND STUDY OF PHOTOCATALYTIC ACTIVITY OF PVA CAPPED ZINC INDIUM SELENIDE NANOPARTICLES UNDER UV LIGHT IRRADIATION USING METHYL RED DYE
Abstract: In this work, we report the structural morphology, optical properties and photocatalytic activity of polymer capped zinc indium selenide nanoparticles, which have been synthesized by solvothermal method. PVA is acted as capping agent. The PVA capped zinc indium selenide nanoparticles were characterized using XRD, SEM with EDAX, AFM, TEM and UV-Vis absorption spectroscopy. The structural properties of PVA capped zinc indium selenide nanoparticles have been characterized by X-ray diffraction (XRD) …
Published in International Journal of Polymer Science and Engineering · Vol. 5, Issue 1, 2019 · pp. 41–51 Read article
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Synthesis and Characterization of Quinacridone Violet (Pigment Violet 19): Process Optimization and Colorimetric Evaluation
Abstract: Objective: This study focuses on the synthesis and characterization of Quinacridone Violet (Pigment Violet 19), a high-performance organic pigment known for excellent lightfastness and durability. The research aims to optimize the manufacturing process and evaluate the colorimetric properties of the synthesized pigment. Methods: PV 19 was synthesized via a multi-step process involving condensation, oxidation/hydrolysis, and ring closure/cyclization reactions. Two experimental batches (MM#973-A1/B1 and MM#974-A1/B1) were prepared with varying mole ratios …
Published in International Journal of Polymer Science and Engineering · Vol. 12, Issue 1, 2026 · pp. 41–51 Read article
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Green approach for the synthesis of Titanium dioxide nano particles and their characterization
Abstract: The ecofriendly and sustainable method of green synthesis of nanoparticles gained a lot of popularity these days. Azadirachta indica (neem) leaves are used in this study to identify the eco friendly synthesis of titanium dioxide nanoparticles (TiO 2 NPs). TiO 2 NPs can be easily and sustainably synthesized from titanium precursors using neem leaves having bioactive compounds. Green production of TiO 2 NPs is facilitated by the stabilizing and capping …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 11, Issue 1, 2026 · pp. 50–58 Read article
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Structural, Optical, and Antibacterial Properties of NiCr₂O₄/NiO Nanocomposite Synthesized by a Facile Microplasma Electrochemical Process
Abstract: Nowadays increasing severity of environmental pollution and antibiotic resistance poses significant global challenges, particularly due to the accumulation of organic pollutants from industrialization and the proliferation of antibiotic-resistant bacteria, which jeopardize ecosystems and public health. To address these issues, the development of advanced nanocomposites with photocatalytic and antimicrobial properties is of paramount importance. This article reports the synthesis of NiCr₂O₄/NiO nanocomposite conducted in the current study via atmospheric pressure microplasma …
Published in International Journal of Composite and Constituent Materials · Vol. 10, Issue 2, 2024 · pp. 1–12 Read article
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Seaweed Mediated Biosynthesis of Silver Nanoparticles Using Gracilaria fergusonii J.Ag. Collected From Hare Island, Thoothukudi in the South East Coast of Tamil Nadu, India
Abstract: In the present study silver nanoparticles were synthesized using the aqueous extract of red seaweed Gracilaria fergusonii J.Ag. as the reducing agent. The formation of silver nanoparticles was confirmed by colour change from light yellow to dark brownish red, UV– visible spectroscopy, FT-IR, X-ray diffraction method (XRD), scanning electron microscopy (SEM) and energy dispersive X-ray microanalysis spectroscopy (EDS). The anoparticles showed an absorbance at 442 nm on UV–visible spectroscopy. The …
Published in International Journal of Plant Biotechnology · Vol. 1, Issue 1-2, 2015 · pp. 50–57 Read article
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Investigation on Synthesis and Evaluation of Nanopore NaA Zeolite Membranes
Abstract: Effects of synthesis parameters on the membrane structure and performance have been investigated for nanopore NaA zeolite membranes grown onto seeded mullite supports. Molar composition of the starting gel of nano NaA membranes was: SiO2/Al2O3=0.8–3.2, Na2O/Al2O3=1.6–4.6, and H2O/Al2O3=50–200. Also, effects of crystallization time and temperature on the membrane performance were studied. X-ray diffraction (XRD) patterns of the membranes exhibited peaks corresponding to the support and the zeolite. The crystal species …
Published in International Journal of Analytical and Applied Chemistry · Vol. 3, Issue 2, 2017 · pp. 9–22 Read article
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Crystal Growth, Synthesis and Characteristic Studies of Bismuth Doped Tristhioureazinc (II) Sulpate (ZTS) Crystal
Abstract: Potential semi organic tristhioureazinc(II) sulphate (ZTS), One of the best room temperature growth techniques for nonlinear optical materials with high SHG efficiency is slow evaporation solution growth, which produces pure and single crystals for use in laser technology and photonic applications. Single crystals Doping of Bismuth fluoride (equimolar) to ZTS is done during the crystallization process is further analysed by single crystal XRD which infers that the Bismuth doped ZTS …
Published in International Journal of Chemical Separation Technology · Vol. 9, Issue 2, 2023 · pp. 45–52 Read article
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Preparation and Evaluation of Nano pore Faujasite Membranes
Abstract: Nano pore Faujasite zeolite membranes were synthesized by in-situ hydrothermal method on porous ceramic tubes. Hydrothermal crystallization was carried out under an autogenously pressure and at a static condition of 100 oC. Molar composition of the starting gel of Faujasite zeolite membranes were NaX: SiO2/Al2O3=10-27, Na2O/Al2O3=4-9, H2O/Al2O3=250; NaY: SiO2/Al2O3=2.5-4, Na2O/SiO2=1.08-2, H2O/Na2O=30-200. X-ray diffraction (XRD) patterns of the membranes exhibited peaks corresponding to the support and the zeolite. The crystal species …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 3, Issue 2, 2017 · pp. 15–24 Read article
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A Comprehensive Characterization of Zinc Chloride: Unveiling its Role as a Hygroscopic Preservative and Drying Agent through Elemental, Structural, and Morphological Analysis
Abstract: This study presents a detailed investigation of Zinc Chloride( )) utilizing the following different analytical techniques, X-ray diffraction(XRD), Electron Dispersive Spectroscope (EDS), Transmission Electron Microscope (TEM), Scanning Electron Microscope (SEM). Zinc Chloride was synthesized using the hydrothermal method. The elemental, structural, morphological, and optical properties of Zinc Chloride ( )) were thoroughly analyzed. The hygroscopic nature and properties of Zinc Chloride upon exposition to air was revealed and its weight/mass …
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 9, Issue 2, 2023 · pp. 13–19 Read article
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Application of Suitable Admixtures (Lime and RHA) for Improvement of Pavement Subgrade
Abstract: Abstract The quality of a pavement depends on the strength of its sub-grade. The present investigation has been carried out with easily available materials like lime and rice husk ash mixed individually and in combinations with different proportions. The different percentages of lime with respect to weight of dry soil were 2%, 4%, 6%, 8% 10% and for rice husk ash (RHA) were 3%, 6%, 9% and 12%. In each …
Published in International Journal of Geological and Geotechnical Engineering · Vol. 1, Issue 2, 2015 · pp. 14–31 Read article